New biopolymer nanocomposites-based Polycaprolactone /polybutylene succinate modified clay: preparation and characterization

M. Al-Mosawy
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Abstract

(Polybutylin succinate)PBS / (Polycaprolactone)PCL and AZO from organic clays incorporating2-(diethylamino)ethyl 3-((4acetylphenyl)diazenyl)-4-aminobenzoate montmorillonite (AZO-MMT) were used to produce polymer compounds by mixing the solution. These materials have been characterized using X-ray diffraction, infrared spectroscopy (FTIR), thermogravimetric analysis (TGA) and transmission electron microscopy (TEM). The nanocomposites have shown increased thermal stability. Where the results obtained from the XRD indicate that the materials prepared in this research are nanocomposites. The results of TEM were confirmed by the insertion of the nanocomposite. In addition, the solution molding process was used to prepare these nanocomposites, and these results were distinguished for comparison with the above-
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新型生物高分子纳米复合材料聚己内酯/聚丁二酸酯改性粘土的制备与表征
用有机粘土中2-(二乙基氨基)乙基3-((4乙酰苯基)二氮基)-4-氨基苯甲酸蒙脱土(AZO- mmt)混合的PBS /(聚己内酯)PCL和AZO制备聚合物化合物。利用x射线衍射、红外光谱(FTIR)、热重分析(TGA)和透射电子显微镜(TEM)对这些材料进行了表征。纳米复合材料表现出更高的热稳定性。XRD测试结果表明,所制备的材料为纳米复合材料。纳米复合材料的插入证实了TEM的结果。此外,采用溶液成型工艺制备了这些纳米复合材料,并将这些结果与上述结果进行了比较
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