Effect of microwave sintering on structural and magnetic properties of SrFe12O19 nanopowders

S. Katlakunta, S. Meena, R. S. Shinde, S. Murthy
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Abstract

Nanocrystalline SrFe12O19 has been prepared by microwave hydrothermal method at 473 K/90 min, subsequently annealed at different temperatures using microwaves (2.45GHz). The average particle size of the powders was found to be 48 nm. The plate shape grains were observed in FE-SEM at 1073 K. The crystals exhibited the typical hexagonal ferrite growth habit with a plate-like geometry. The effects of microwave sintering temperature on crystallinity, morphology and magnetic properties have been investigated. The grain sizes of sintered hexaferrites are in the range of 250 to 890 nm. The value of Ms = 58 kA/m and Hc = 125 kA/m was obtained at 1173 K/1h.
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微波烧结对SrFe12O19纳米粉体结构和磁性能的影响
采用微波水热法制备了SrFe12O19纳米晶,加热温度为473 K/90 min,然后采用微波(2.45GHz)在不同温度下进行退火。粉末的平均粒径为48 nm。在1073 K的FE-SEM中观察到板状晶粒。晶体表现出典型的六方铁氧体生长习性,具有板状几何结构。研究了微波烧结温度对材料结晶度、形貌和磁性能的影响。烧结后的六铁素体晶粒尺寸在250 ~ 890nm之间。在1173 K/1h下得到Ms = 58 kA/m, Hc = 125 kA/m。
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