{"title":"The effect of Ni on the cryogenic attritor milling of Metglas Fe78B13Si9","authors":"B Huang , H.G Jiang , R.J Perez , S.R Nutt , E.J Lavernia","doi":"10.1016/S0965-9773(00)00428-1","DOIUrl":null,"url":null,"abstract":"<div><p><span>The addition of 17 at.% of elemental Ni powders to the cryogenic attritor milling of Metglas Fe</span><sub>78</sub>B<sub>13</sub>Si<sub>9</sub> slowed the mechanical crystallization of the α-Fe and Fe<sub>2</sub><span>B phases. Transmission electron microscopy<span> (TEM) observation and energy dispersive spectroscopy (EDS) analysis indicated that no more than 3.60 at.% of Ni dissolved into the Metglas, which was well within the equilibrium solubility limit of Ni in α-Fe. It is proposed that the addition of Ni impede mechanical crystallization during attritor milling by inhibiting bending and wear-like processes which could otherwise cause crystallization.</span></span></p></div>","PeriodicalId":18878,"journal":{"name":"Nanostructured Materials","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"1999-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/S0965-9773(00)00428-1","citationCount":"4","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Nanostructured Materials","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0965977300004281","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 4
Abstract
The addition of 17 at.% of elemental Ni powders to the cryogenic attritor milling of Metglas Fe78B13Si9 slowed the mechanical crystallization of the α-Fe and Fe2B phases. Transmission electron microscopy (TEM) observation and energy dispersive spectroscopy (EDS) analysis indicated that no more than 3.60 at.% of Ni dissolved into the Metglas, which was well within the equilibrium solubility limit of Ni in α-Fe. It is proposed that the addition of Ni impede mechanical crystallization during attritor milling by inhibiting bending and wear-like processes which could otherwise cause crystallization.
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