Novel synthesis of ultrafine hourglass-shaped aluminum hydroxide particles

Qiuling Zhou, Ling Zhang, Chunzhong Li, Wei Shao
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引用次数: 3

Abstract

In a novel method for synthesizing ultrafine aluminum hydroxide particles presented in this paper, the morphology and crystal structure of the particles were investigated by TEM, XRD, etc. The process consisted of two steps: chemical precipitation by acid and carbonation. The product has an hourglass or half-hourglass morphology with a narrow size distribution of 150-200 nm. Major endothermal peak of decomposition was found at 270°C by differential thermal analysis. X-ray diffraction identified the product as bayerite. Those properties were compared with those of aluminum hydroxide prepared by carbonization only.

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超细沙漏状氢氧化铝颗粒的新合成方法
本文提出了一种合成超细氢氧化铝颗粒的新方法,利用TEM、XRD等手段对颗粒的形貌和晶体结构进行了研究。该工艺包括两个步骤:酸化学沉淀和碳酸化。该产品具有沙漏或半沙漏形态,尺寸分布在150- 200nm之间。差热分析发现,270℃为主要的吸热峰。x射线衍射鉴定产物为拜耳石。并与炭化法制备的氢氧化铝进行了比较。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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