快速烧结高半透明氧化锆陶瓷的耐老化性能。

IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Journal of oral science Pub Date : 2023-01-11 DOI:10.2334/josnusd.22-0264
Min Yan, Shinn-Jyh Ding, Cheng-Wei Lin, Cian-Li Wei, Yi-Wen Huang, Chun-Chuan Yang
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引用次数: 3

摘要

目的:快速烧结技术已成为缩短氧化锆修复体制作时间的最直接方法之一。本研究旨在探讨快速烧结5mol %钇-部分稳定氧化锆(5Y-PSZ)的耐老化性能。方法:采用两种5Y-PSZ材料,分别进行快速烧结(RS)和常规烧结(CS)。体外时效5 h后,进行形貌观察、晶粒尺寸测定和相组成分析。通过双轴、三点弯曲试验和维氏显微硬度试验评估了其力学性能。结果采用3-way ANOVA分析。结果:RS组和CS组均具有致密的显微结构。烧结方式和时效方式的相互作用影响了氧化锆陶瓷的晶粒尺寸。两组时效后均呈现出相同的立方相特征峰。无论采用何种烧结方法,老化前后被测氧化锆的力学性能均无显著差异。结论:快速烧结5Y-PSZ材料具有与常规烧结材料相似的显微组织、相组成和力学性能。两种烧结方法制备的材料在时效后的性能没有明显变化。
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Aging resistance of highly translucent zirconia ceramics with rapid sintering.

Purpose: Rapid sintering technology has become one of the most direct methods for shortening the manufacturing time of zirconia restorations. This study aimed to explore the aging resistance of rapid-sintered 5 mol% yttria-partially-stabilized zirconia (5Y-PSZ).

Methods: Specimens were made from two types of 5Y-PSZ material and subjected to rapid sintering (RS) and conventional sintering (CS). After in vitro aging for 5 h, morphology observation, grain size measurement, and phase composition analysis were performed. The mechanical properties were evaluated by biaxial, three-point flexural tests, and the Vickers microhardness test. Results were analyzed by 3-way ANOVA.

Results: Both the RS group and the CS group had a dense microstructure. The tested zirconia ceramics had different grain sizes, which were affected by the interaction between the sintering method and aging. Both groups revealed the same characteristic peaks of the cubic phase after aging. Regardless of the sintering method used, there was no significant difference in the mechanical properties of the tested zirconia before and after aging.

Conclusion: The rapid-sintered 5Y-PSZ materials had a microstructure, phase composition and mechanical properties similar to those of conventional sintered materials. The characteristics of the materials prepared using the two sintering methods did not change significantly after aging.

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来源期刊
Journal of oral science
Journal of oral science DENTISTRY, ORAL SURGERY & MEDICINE-MATERIALS SCIENCE, BIOMATERIALS
CiteScore
3.80
自引率
0.00%
发文量
58
期刊介绍: Information not localized
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