激光烧结钨铼合金的组织与性能

Jiang Shan
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引用次数: 0

摘要

采用激光烧结法制备了添加铼和钽的钨合金。采用光学显微镜、x射线衍射仪和显微硬度计对样品的组织和性能进行了测试。通过调节激光束功率和激光光斑扫描速度,制备了致密钨合金块材。通过脱附脱氧预处理和惰性气体保护可避免粉末氧化。激光烧结过程中存在静态再结晶现象。在样品的核心处,形成了明显大于粉末颗粒的等轴颗粒。在试样边缘由于散热而温度低于芯部的地方,形成了小而不成熟的等轴晶粒,晶粒尺寸接近粉末的粒度。钽和铼的加入在钨中形成了固溶体。由于固溶体原子对晶格的影响,随着钽和铼添加量的增加,样品的密度降低,显微硬度相应提高。
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Microstructure and Properties of Tungsten Rhenium Alloy Prepared by Laser Sintering
Tungsten alloy with addition of rhenium and tantalum was prepared by laser sintering. Microstructure and properties of the samples were tested by optical microscope, X-ray diffractometer and microhardness tester. Dense tungsten alloy block materials were prepared by adjusting laser beam power and laser spot scanning speed. The oxidation of powder can be avoided by desorption and deoxygenation pretreatment and inert gas protection. Static recrystallization occurred in the laser sintering process. In the core of the sample, equiaxed grains significantly larger than the powder particles were formed. In the edge of the sample, where the temperature was lower than the core due to heat dissipation, small and immature equiaxed grains whose size was close to the particle size of the powder were formed. The addition of tantalum and rhenium formed a solid solution in tungsten. Because of the effect of solid solution atoms to the lattice, with the increase of the addition of tantalum and rhenium, the density of samples decreased, while the microhardness increased accordingly.
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