不同配比制备的壳聚糖/聚丙烯腈共混物的抗菌活性

H. Mahmood, M. Jawad
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引用次数: 6

摘要

摘要采用溶液浇铸法制备了不同PAN质量比(1、2、3、4、5%)的壳聚糖和壳聚糖:PAN共混物。通过x射线衍射(XRD)、傅里叶变换红外光谱(FTIR)和应变应力测试对制备的样品进行了结构和力学性能测试。XRD测量结果表明,共混物的形成是由平面间距离的变化引起的。此外,多糖的某些FTIR波段能量的变化和强度的降低表明壳聚糖:PAN共混物的形成。当PAN比为1%时,拉伸强度最大。用抑菌浓度法考察了壳聚糖/PAN共混物的抑菌活性。结果表明,不同样品的活性等级不同。壳聚糖/聚丙烯腈共混物的抑菌率在1%时最高。与革兰氏阴性菌相比,该混合物对革兰氏阳性菌的效果较差。采用溶液浇铸法制备了不同PAN质量比(1、2、3、4、5%)的壳聚糖和壳聚糖:PAN共混物。通过x射线衍射(XRD)、傅里叶变换红外光谱(FTIR)和应变应力测试对制备的样品进行了结构和力学性能测试。XRD测量结果表明,共混物的形成是由平面间距离的变化引起的。此外,多糖的某些FTIR波段能量的变化和强度的降低表明壳聚糖:PAN共混物的形成。当PAN比为1%时,拉伸强度最大。用抑菌浓度法考察了壳聚糖/PAN共混物的抑菌活性。结果表明,不同样品的活性等级不同。壳聚糖/聚丙烯腈共混物的抑菌率在1%时最高。这种混合物对革兰氏阳性细菌的效果不如革兰氏阴性细菌。
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Antibacterial activity of chitosan/PAN blend prepared at different ratios
Abstract. Chitosan and Chitosan: PAN blend with different PAN weight ratios (1, 2, 3, 4 and 5%) were prepared by solution casting method. The structural and mechanical properties for prepared samples were done by X-ray diffraction (XRD), Fourier transformed infrared spectroscopy (FTIR) and strain stress test. The XRD measurements indicate the formation of the blend by the variation of inter-planer distances. Also, the shift in some FTIR bands energy for polysaccharides and reduce their intensities indicate the formation of Chitosan:PAN blend. The largest tensile appeared at 1% PAN ratio. The chitosan/PAN blends were examined their antibacterial activity using the inhibition concentration method. The results show different grades of activity at the different samples. The highest inhibition of the bacteria for Chitosan/PAN blend at a 1% blend ratio. The blend has less effectiveness against gram-positive bacteria than gram-negative.Abstract. Chitosan and Chitosan: PAN blend with different PAN weight ratios (1, 2, 3, 4 and 5%) were prepared by solution casting method. The structural and mechanical properties for prepared samples were done by X-ray diffraction (XRD), Fourier transformed infrared spectroscopy (FTIR) and strain stress test. The XRD measurements indicate the formation of the blend by the variation of inter-planer distances. Also, the shift in some FTIR bands energy for polysaccharides and reduce their intensities indicate the formation of Chitosan:PAN blend. The largest tensile appeared at 1% PAN ratio. The chitosan/PAN blends were examined their antibacterial activity using the inhibition concentration method. The results show different grades of activity at the different samples. The highest inhibition of the bacteria for Chitosan/PAN blend at a 1% blend ratio. The blend has less effectiveness against gram-positive bacteria than gram-negative.
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