硫脲对l -脯氨酸氯化镉单晶影响的研究

Jaslin J. Christopher, A. Jebamalar, J. Beena
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引用次数: 0

摘要

采用室温慢蒸发法制备了纯和掺硫脲的l -脯氨酸一水氯化镉单晶。SXRD分析给出了晶格参数和晶体体系的详细信息。EDAX谱证实了掺杂单晶中存在C、H、S、Cd、Cl。FTIR分析证实标题材料中存在各种官能团。紫外透射光谱证实了掺杂晶体透明度的增加。标题材料的绿光发射是通过荧光分析确定的。力学分析表明,硫脲掺杂l -脯氨酸氯化镉一水合物属于软材料范畴,掺杂晶体的二次谐波效率是KDP的0.8倍。
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Investigation on the Impact of Thiourea on L-Proline Cadmium Chloride Single Crystal
Pure and thiourea doped single crystals of L-proline cadmium chloride monohydrate were grown by slow evaporation method at room temperature. The SXRD analysis gives the details about the lattice parameters and crystal system. EDAX spectrum corroborated the incorporation of C, H, S, Cd, Cl in doped single crystal. FTIR analysis confirms the presence of various functional groups in the title material. The UV transmittance spectrum confirms the increase in transparency of the doped crystal. The green light emission of the title material was attributed by fluorescence analysis. The mechanical analysis suggests that thiourea doped L-Proline cadmium chloride monohydrate comes under soft material category and the second harmonic efficiency of doped crystal was 0.8 times than KDP.
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