光学层的清洗效果:误差特征及分析方法

E. M. Zambrano, C. Wünsche, L. Mechold, S. Herr
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摘要

在高性能光学元件需求不断增长的过程中,介质镀膜工艺是光学元件精细化、保证其功能性的关键技术。这些光学器件基于光学干涉涂层,由高、低折射率材料的透明单层交替堆叠而成。假设浊度和涂层中嵌入的缺陷被认为是限制光学涂层质量的主要因素,那么涂层前对基材的清洁水平必须非常高。特别重要的是层堆和基板之间的界面,特别是在制造过程中从玻璃表面过渡到涂层期间的相互作用。这种相互作用被认为是由抛光、储存期间的腐蚀或涂层前基材清洗过程中的影响引起的。因此,有必要描述每种类型的缺陷,并定义哪种技术足以有效地分析它们中的每一种。该项目旨在提高人们对涂层过程中发生的事情的认识和知识,特别是在制造过程中了解基材的物理过程。在分析了物料流之后,首先将重点放在清洗程序上。假设化学清洗是影响界面缺陷的主要因素之一。由于外部成分的额外影响和洗脸盆温度的升高,玻璃基板表面可能发生化学反应。
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Cleaning effects in optical layers: error characteristics and analysis methods
In the course of the ever-increasing demand of high-performance optical components, dielectric coating processes are the key technology for the refinement of optics, ensuring their functionality. These optics are based on optical interference coatings, which are formed by a layer stack of alternating transparent single layers of high and low refractive index material. Assuming that turbidity as well as defects embedded in coatings are considered as a primary factor limiting the quality of optical coatings, the level of cleaning the substrates before coating has to be extremely high. Particular importance is attached to the interface between the layer stack and the substrate, especially to the interaction during the transition from the glass surface to the coating during the manufacturing process. This interaction is assumed to be caused by polishing, by corrosion during storage time or by effects during cleaning of the substrate before coating. Thus, it is necessary to characterize each type of defect and to define which technique is adequate to analyze each one of them efficiently. The project aims to raise the awareness and knowledge in terms of what happens during the coating process and, in particular, to understand the physical processes at the substrate during the manufacturing process. After analyzing the material flow, first focus was set on the cleaning procedure. It is assumed that one of the main influences on defects in the interface is the chemical cleaning. Chemical reactions on the surface of the glass substrate may occur due to additional effects of external components and elevated temperature in the washing basins.
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