用氢氧化钾化学活化从细菌纤维素中提取活性炭

Chinwaranon Boongate, M. Phisalaphong
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引用次数: 4

摘要

本研究以细菌纤维素(BC)为碳源制备活性炭。以氢氧化钾(KOH)为活化剂,通过一步化学活化法制备BC活性炭,考察了活化温度400、500、600、700℃对活性炭性能的影响。采用傅里叶变换红外光谱(FTIR)、x射线粉末衍射(XRD)和扫描电镜(SEM)对活性炭的化学性质、结构和形貌进行了表征。结果表明,用KOH活化BC制备的活性炭具有高比表面积和大孔体积。在400 ~ 500℃的炭化温度下,得到了比表面积和孔体积最大的活性炭。随着活化温度升高至700℃,孔隙结构被破坏。
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Activated carbons from bacterial cellulose by chemical activation with potassium hydroxide
In this study, bacterial cellulose (BC) was used as carbon source for preparing activated carbons. Activated carbon from BC was prepared in a one-step chemical activation process by using potassium hydroxide (KOH) as activating agent for 1 h. The influence of activation temperatures, 400, 500, 600 and 700 °C on the characteristics of active carbon was investigated. The activated carbons derived from BC were characterized for chemical property, structure and morphology by Fourier transforms infrared (FTIR) spectroscopy, X-ray powder diffraction (XRD) and Scanning electron microscope (SEM). It was shown that the activated carbons prepared from BC using KOH activation have high surface area and large pore volumes. Activated carbon with the highest surface area and pore volume was obtained at the carbonization temperature of 400-500 °C. It was found that the pore structure was destroyed with increasing activation temperature to 700 °C.
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