凤尾草(Neriumoleander) L.和绵草(Lantana camara)有效成分的植物化学筛选与鉴定

O. Abdelgabar, Ehab E. M. Alias, Y. O. Assad
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引用次数: 0

摘要

对夹竹桃叶粉和山楂叶粉进行了皂苷、苷类、萜烯类、黄酮类、单宁类、生物碱类、心苷类和氰苷类的检测。定性分析和植物化学筛选结果表明,夹竹桃叶提取物中大部分天然产物均存在,而夹竹桃叶提取物中除皂苷和苷外,其余天然产物均存在。采用气相色谱-质谱联用技术对夹竹桃叶乙醇提取物和夹竹桃叶乙醇提取物的化学成分进行了研究。对夹竹桃叶乙醇提取物进行分析,鉴定出22种成分,其中4-0-甲基甘露糖、角鲨烯、正十六酸、维生素E;3, 5-dimethoxyacetophenone;9、12、15-十八烯三酸和2,3 -二氢苯并呋喃含量分别为35.92%、14.72%、11.10%、7、57%、7.13%、6.84%、3.19%,其余含量为1.3 ~ 1.97%。主要化学成分有42种,其中石竹烯(3,1,0)己烷、4-亚甲基-1-(1-甲基-l - ululene)、石竹烯(3,1,0)己烷-6-甲醇、2-hydro、桉叶醇、石竹烯氧化物分别占21.47%、11.68%、10.93%、9.75%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%、8.97%。其余成分的含量范围为0.1.1 ~ 3.53%。
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Phytochemical Screening and Identification of Active Ingredients in Nerium (Nerium oleander) L. and Lantana (Lantana camara)
Powdered leaves of Nerium oleander L. and Lantana camara were screened for detection of saponins, glycosides, terpenes, flavonoids, tannins, alkaloids, cardiac glycosides, and cyanogenic glycosides. The results of the qualitative analysis and phytochemical screening profiles indicated that, most of the natural tested products are presented in N. oleander L leave extracts, for L. camara, most of the natural products tested for are present except saponins and glycosides. The chemical compositions of the leaf ethanol extract of N. oleander and L. camara were investigated using gas chromatography –mass spectroscopy (GC-MS). Analysis of N.oleander leaf ethanol extract revealed the existence of twenty two components identified, of them 4-0-methylmannose, Squalene, n-hexadecanoic acid, vitamin E; 3,5-dimethoxyacetophenone; 9,12,15-octadecatrienoic acid and benzofuran-2, 3-dihydro, represent 35.92%, 14.72%, 11.10%, 7,57%, 7.13%, 6.84 %, 3.19%, respectively, the other components were ranged from 1.3 to 1.97 %. While L. camara major chemical component were found to be forty two of them, caryophyllene bicycle (3, 1, 0) hexane, 4-methylene-1-(1-methyl-lhumulene, bicycle (3, 1, 0) hexane-6-methanol,2-hydro, eucalyptol, caryophyllene oxide, represent 21.47%,11.68 %,10.93 %,9.75% 8.97%, 8..03%, respectively, the other components were ranged from ,1.1 to 3.53 % .
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