硅衬底上电沉积多壁碳纳米管薄膜的表征

M. Rahman, M. A. Uddin, Ahmedullah Aziz, Tanvir Mustofa, Z. Mahmood, T. Soga, S. M. Mominuzzaman
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引用次数: 3

摘要

在硅衬底上沉积了多壁碳纳米管(MWCNT)薄膜。研究了0.1%和0.2%甲醇掺入MWCNT溶液的效果。分析了不同溶液沉积前后的pH值。溶液沉积后pH值升高。观察到电流密度随外加电位的变化。电流密度随MWCNT含量的增加而增加。采用扫描电镜(SEM)、紫外可见红外光谱(UV-VIS-IR)和拉曼光谱(Raman spectroscopy)对电沉积MWCNT薄膜进行了表征。在SEM显微照片中,与纯Si衬底相比,电沉积薄膜发生了变化。拉曼测量证明了MWCNT在这些薄膜中的无定形性质。紫外-可见-红外测量结果表明,纳米碳纳米管的增加增加了对光的吸收。因此,在硅衬底上电沉积MWCNT薄膜的光电性能是可调的。
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Characterization of electrodeposited multiwall carbon nanotube films on silicon substrates
Multiwall Carbon Nanotube (MWCNT) films were deposited on Silicon (Si) substrate. The effect of 0.1% and 0.2% solutions of MWCNT incorporation with methanol were investigated. pH of various solutions before and after deposition has been analyzed. pH of the solutions was increased after deposition. Change in the variation of current density as a function of applied potential was observed. Current density was increased as the percentage of MWCNT was increased. The electrodeposited MWCNT films were characterized by SEM, UV-VIS-IR and Raman spectroscopy. In SEM micrographs, changes were observed in the electrodeposited films compared to pure Si substrates. Raman measurement proved the amorphous nature of MWCNT in these thin films. From the UV-VIS-IR measurement it was observed that the absorption of light has been increased by the increase of MWCNT. So the optoelectronic properties of the electrodeposited films are tunable by electrodeposition using MWCNT on Si substrates.
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