碳纳米管/聚乙烯醇纳米复合材料的合成及电学、热学和形貌表征

Gulfam Nasar, Uzma Khalil, Muhammad Saleem Khan, Qaisar Nadeem
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引用次数: 1

摘要

目前这项工作的目标是为纳米科学和纳米技术带来一种有用的物质,这种物质可能是离子储存的“问题解决者”。在水介质中制备了五种浓度的碳纳米管/聚乙烯醇纳米复合材料。利用交流阻抗谱、差热分析、热重分析(TG/DTA)和扫描电子显微镜(SEM)对纳米复合材料进行了表征。用阻抗谱法测定了纳米复合材料的离子电导率。CNT/PVA纳米复合材料的电导率比CNT或PVA低。TG/DTA图表现出规律的模式,显示热稳定性增加。制备样品的SEM形貌显示了良好的聚合物-填料在界面的形态排列,这表明聚合物与填料之间具有良好的相容性。
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Synthesis and Characterization of CNT/PVA Nanocomposites for Electrical, Thermal and Morphological Properties
The goal of the current work is to bring a helpful substance to nanoscience and nanotechnology that might be a "problem solver" for ion storage. Carbon nanotubes/ PVA nanocomposites were prepared in five concentrations in aqueous medium following film formation. The resulting nanocomposites were characterized using “AC Impedance Spectroscopy, Differential Thermal Analysis, Thermal Gravimetric Analysis / (TG/DTA) and Scanning Electron Microscopy (SEM)”. Ionic conductivity of the nanocomposites was determined from impedance spectroscopy. CNT/PVA nanocomposites exhibited lower conductivity as compared with CNT or PVA separately. TG/DTA graphs exhibited a regular pattern, showing an increase in the thermal stability. Morphology of the prepared samples as shown by SEM reveals a favourable polymer-filler morphological arrangement at the interphase, which is suggestive of a favourable compatibility between the polymer and the filler substance.
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