真空钎焊钛/316L不锈钢过渡接头在超导射频腔氦容器中的应用

P. Ganesh, Abhay Kumar, S. Vishwakarma, A. Bose, R. Gupta, B. Sindal, S. Rai, P. C. Rao, P. R. Sankar, D. Nagpure, R. Kaul, G. Mundra, B. Singh
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摘要

超导射频(SRF)空腔将成为印度散裂中子源和加速器驱动系统的重要组成部分。高β 650兆赫SRF腔将被封闭在一个圆柱形容器中,以容纳液氦(LHe)。钛(Ti)被认为是建造氦容器的材料。氦气容器的氦气进口供应管路和回氦气管路采用316L不锈钢(SS)制造。这需要Ti和316LSS之间的双金属管状过渡接头,在LHe温度下工作。真空钎焊和爆炸焊接是连接这两种不同金属的潜在方法,因为熔焊会导致广泛的开裂。本试验采用BVAg8钎焊填充金属(BFM)真空钎焊连接Ti-pipe/316LSS法兰。该工艺的显著特点包括:(i)在SS部件上电镀5-10 μm镍作为扩散屏障,防止铁向钛的可能迁移,同时提高BFM的表面润湿性;(ii)使用304 SS塞,收缩配合ti管,在加工过程中实现ti管的尺寸和轮廓精度,同时控制钎焊过程中的连接间隙。钎焊接头显示出均匀的接头厚度和可接受的密封性水平(氦泄漏率2 × 10-10mbar.lit/s),并且在293 K和77 K之间持续了6次热循环。夹层结构的Ti- ss钎焊试样的抗剪强度在50 ~ 60 MPa之间,破坏发生在Ti/钎焊界面。
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Vacuum Brazing Of Titanium/316L Stainless Steel Transition Joint For Application In Helium Vessel Of Superconducting RF Cavities
Superconducting radiofrequency (SRF) cavities would form important part of the proposed Indian Spallation Neutron Source and Accelerator Driven System. The high beta 650 MHz SRF cavity would be enclosed in a cylindrical vessel to hold liquid helium (LHe). Titanium (Ti) is being considered as the material of construction of helium vessel. The LHe inlet supply line and return helium gas pipe line of the helium vessel would be made of 316L stainless steel (SS). This requires a bi-metallic tubular transition joint between Ti and 316LSS, operating at LHe temperature. Vacuum brazing and explosive welding are potential processes for joining these two dissimilar metals, as fusion welding leads to extensive cracking. In the present experimental study, vacuum brazing was performed to join Ti-pipe/316LSS flange with BVAg8 braze filler metal (BFM). Notable features of the process include use of (i) 5-10 μm nickel electro-plating as a diffusion barrier on SS part for preventing possible iron migration towards titanium while improving surface wettability for BFM and (ii) use of 304 SS plug, shrunk fit into Ti-pipe, for achieving dimensional and profile accuracy of Ti-pipe during machining while also controlling joint gap during brazing process. The brazed joint displayed uniform joint thickness and acceptable level of hermeticity (helium leak rate 2 x 10-10mbar.lit/s) and also sustained six thermal cycles between 293 K and 77 K. Shear strength of Ti-SS brazed specimens, made in sandwich configuration, was found to be in the range of 50-60 MPa, with failure occurring at Ti/braze interface.
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