芯片上石墨烯-碳糊实验室低功耗化学传感的微型恒电位器

K. Ugsornrat, Triwit Phurksasukkasem, A. Sappat, C. Sriprachuabwong, C. Karuwan, A. Tuantranont
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摘要

本课题研究了便携式电化学测量用微型恒电位器的研制。该微型恒电位器是为实验室芯片上低浓度物质的电化学值分析而制造的。微型恒电位器采用电子电路设计,集成电路制作,单片机控制。芯片实验室设计为t型,利用数字微流体作用于微流体,使液滴移动到芯片实验室的电化学传感器上。该传感器由丝网印刷电极组成:石墨烯-碳糊工作电极和反电极以及银/氯化银糊参比电极。采用丝网印刷法制备了电化学电极。对微型恒电位器进行了标定,用于电化学传感器的测试。为了进行分析,对芯片上的实验室进行了低浓度测试,使用六氰高铁酸钾,并将最小试剂消耗的浓度从200 mM增加到1000 mM,增加200 mM。这种微型恒电位器可以有效地区分低浓度物质的浓度
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Mini-Potentiostat for Low Power Chemical Sensing of Graphene-Carbon Paste Lab on a Chip
This research studied the development of mini-potentiostat for portable electrochemical measurement. The mini-potentiostat was fabricated for analysis of electrochemical values with substances in low concentrations to use with lab on a chip. The mini-potentiostat was designed by using electronic circuits and fabricated from integrated circuits and controlled by microcontrollers. The lab on a chip was designed to be T-shaped and uses digital microfluidics for acting on microfluid to move the liquid droplets to electrochemical sensor of lab on a chip. The sensor consists of screen-printing electrodes: a graphene-carbon paste working and counter electrodes and a silver/silver chloride paste reference electrode. The electrochemical electrodes were fabricated by screen printing methods. The mini-potentiostat was calibrated to test for electrochemical sensor. For analysis, the lab on a chip was tested using low concentration, using potassium hexacyanoferrate and varying concentration of minimal reagent consumption from 200 mM to 1000 mM with increment of 200 mM. This mini-potentiostat can distinguish the concentration of substances with low concentrations effectively
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