ZnO纳米片与MEMS平台的集成及其在气体传感器中的应用

P. Bhattacharyya, Sunipa Roy, C. Sarkar
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引用次数: 1

摘要

与传统陶瓷气体传感器相比,基于MEMS的气体传感器由于其低功耗,高灵敏度,更快的响应和与CMOS电路的兼容性而具有优越的性能。微加热器在薄膜MEMS结构上的设计是实现所需温度的关键。本文利用Intellisuite v8.2设计了一种曲线形微加热器,并在微加工硅平台(2mm×2mm)上采用镍合金(DilverP1)制作。采用低温化学沉积技术(使用锌酸钠浴)将传感层沉积在微加热器的顶部。用FESEM研究了ZnO的结构形貌。形成了平均尺寸为50 ~ 70nm的六角形纳米片状结构。采用电阻平面触点(Au-Au),以N2为载气,测试了该器件在不同偏置电压(0-3V)和不同工作温度(30-210℃)下的感氢性能。在H2浓度为20000ppm时,最佳工作温度为~ 150℃,响应幅度为~80.7%,响应时间为~29.6s。在较低的浓度水平(100ppm)下,传感器性能也很好,RM为~36.8%,响应时间为40.8s。
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Integration of ZnO nanoflakes with MEMS platform and its application as gas sensor
MEMS based gas sensors offer superior performance compared to conventional ceramic gas sensors owing to their low power consumption, high sensitivity, faster response and compatibility to CMOS circuits. The design of microheater on the thin membrane of the MEMS structure is crucial to achieve the required temperature. In this paper a meander shaped microheater has been designed using Intellisuite v8.2 and fabricated using a nickel alloy (DilverP1) on micromachined silicon platform (2mm×2mm). A low temperature chemical deposition technique (using Sodium Zincate bath) has been adopted to deposit the sensing layer on top of the microheater. Structural morphology of ZnO was studied by FESEM. The hexagonal nanoflake like structures having average size of 50-70nm were formed. Resistive planar contacts (Au-Au) have been taken and the device was then tested for its hydrogen sensing property at different bias voltages (0-3V) and with different operating temperatures (30-210 °C) taking N2 as a carrier gas. The optimum operating temperature was found ~ 150°C with a high response magnitude of ~80.7% and appreciably fast response time ~29.6s at a H2 concentration of 20000ppm. At lower concentration level (100ppm) the sensor performance was also found to be promising with RM of ~36.8% and response time of 40.8s.
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