一种试扫描原子探针及微针尖阵列尖端处的场分布

O. Nishikawa, Y. Numada, M. Iwatsuki, S. Aoki, Y. Ishikawa
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引用次数: 0

摘要

仅给出摘要形式,如下。通过对低温特高压扫描隧道显微镜(STM)的改造,构建了一个实验扫描原子探针(SAP)。将传统STM的样品支架替换为由10微米厚Pt箔制成的提取电极支架。试样微尖阵列安装在压电管的一端,允许人们以亚纳米精度移动试样。连接低温冰箱冷端和压电管支架的银箔将试样和压电组件冷却至50k。场发射电子和场电离气体离子以原子分辨率投射微针尖阵列单个针尖的图像,场蒸发的针尖原子通过屏幕中心的探针孔飞入反射质分析器的飞行空间。报道了初步实验结果。在构建SAP时,计算了提取电极尖端周围的场分布,以考察场发射电流随提取电极尖端和开孔相对位置的变化。给出了计算的场分布,并将观测到的发射电流变化与相对位置进行了比较。
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A trial scanning atom probe and field distribution at a tip apex of a micro-tip array
Summary form only given, as follows. A trial scanning atom probe (SAP) was constructed by modifying a low temperature UHV scanning tunneling microscope (STM). The specimen holder of the conventional STM was replaced with a holder of an extraction electrode made of a 10 micrometer thick Pt foil. The specimen micro-tip array is mounted at one end of a piezo tube which allows one to move the specimen with subnanometer precision. Silver foils connecting the cold end of the cryogenic refrigerator and the holder of the piezo tube cool the specimen and piezo assembly down to 50 K. Field emitted electrons and field ionized gas ions project images of an individual tip apex of a micro-tip array at atomic resolution and field evaporated apex atoms fly into the flight space of a reflectron mass analyzer through the probe hole at the center of the screen. The results of preliminary experiments are reported. While constructing the SAP, the field distributions around the tip apex were computed in order to examine the variation of field emitted current with the relative position of the tip apex and the open hole of the extraction electrode. The calculated field distribution is presented, comparing the observed variation of emitted current with the relative positions.
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