脱木质素作用时间对竹纤维α -纤维素%收率的影响

J. Sitinjak, H. Nasution, M. Lubis
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摘要

竹纤维(Bambuseae)含有纤维素,可作为复合材料的填料。本研究的目的是通过分离工艺从竹纤维中获得α纤维素。本研究采用NaOH溶剂脱木质素法,在温度为80℃,时间变化为30、60、90、120、180 min的条件下,对竹纤维中α纤维素和其他化合物进行了第一步分离。结果表明,脱木质素的最佳条件为60 min,得率为55.26%。通过对比反应α纤维素上的团簇与竹纤维上的团簇,用FTIR光谱证实了产物(α纤维素)的形成,表明在1641 cm -1吸收区存在以峰形成为特征的纤维素化合物。XRD结果表明,α -纤维素的结晶部分高于α -纤维素本身的非晶态部分,总结晶度指数为93.3%。
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The Effect of Delignification Time on \% Yield of Alpha-cellulose from Bamboo Fiber (Bambuseae) Properties
: Bamboo fiber (Bambuseae) has cellulose content that can be used as a filler in the composites. The objective of this study is to obtain alpha cellulose from bamboo fiber, through the isolation process. This study was carried out using the delignification method with NaOH solvent on temperature at 80 o C and the time variations of 30, 60, 90, 120, 180 minutes as the first stage of separation of alpha cellulose from other compounds contained in bamboo fiber. The results showed that the optimum condition of delignification time was 60 minutes with yield of 55.26%. The FTIR spectra was performed to confirm the formation of the product (alpha cellulose) proved by spectrum indicating the presence of the cellulose compound characterized by peak formation in 1641 cm -1 absorption area by comparing the cluster on the reaction alpha cellulose with the cluster on the bamboo fiber. XRD result showed that the crystalline portion of alpha cellulose was higher than amorf portion of alpha cellulose itself with the total amount of crystallinity index was 93.3%.
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