透射电子显微镜样品台的研制

Kee-Bong Choi, Jaejong Lee, Geehong Kim, Hyungjun Lim, Soongeun Kwon, Sang-Chul Lee
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引用次数: 0

摘要

透射电子显微镜是用来观察和分析膜样品的形态和晶体结构的。样品被放置在一个由电动平台操纵的样品支架上。本研究设计了一种用于透射电子显微镜的样品台。该平台由一个样品支架和四个电动轴组成,用于三个直线运动和一个倾斜运动。特别是,放置在真空环境中的试样必须与大气分离。试样台是在传统试样台的基础上发展起来的。直线运动的运动系统安装在倾斜平台上。电机系统由电机、减速器、编码器、丝杠和直线导轨组成。减速机减速比的选择要满足分辨率的要求。在直线运动中,Y和z运动通过球面关节传递到刀尖。因此,球面关节以杠杆比减小了Y和z运动。带样品的样品架通过导柱转移,将样品置于真空室的中心。样品夹和线性导柱是为气锁设计的。最后进行了实验,验证了研制阶段的性能。
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Development of a Specimen Stage for Transmission Electron Microscopy
A Transmission Electron Microscopy is to observe and to analyze morphology and crystalline structure of a membrane specimen. The specimen is placed onto a sample holder which is manipulated by a motorized stage. In this study, a specimen stage for Transmission Electron Microscopy is designed. The stage consists of a sample holder and four motorized axes for three linear motions and one tilt motion. Especially, the specimen put in a vacuum environment must be separated from the atmosphere. The specimen stage is developed based on the conventional one. The motion systems for the linear motion are put on the tilt platform. The motor system consists of a motor, a reducer, an encoder, a lead screw and a linear guide. The reducing ratio of the reducer is chosen to satisfy the requirement of resolution. Among the linear motions, the Y and Z-motion transferred to the holder tip through a spherical joint. Therefore, the Y and Z-motion is reduced with a lever ratio by the spherical joint. The sample holder with the specimen is transferred through a guide column to put the specimen at the center of the vacuum chamber. The sample holder and the linear guide column are designed for an air-lock. Finally, experiments are carried out to show the performance of the developed stage.
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