电感耦合等离子体发射光谱法测定田间农药中砷含量

Şükrü Kalayci
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引用次数: 2

摘要

本研究用ICP-OES法测定了野药结构中砷的含量。对于砷的分析,土耳其选择了四种不同的常用农药。这些农药在商业上被命名为A、B、C和D样品。采用微波消解法对样品进行适当的溶解处理。砷的测定波长为188.980 nm。ICP-OES首次测定已知酸,灵敏度高。砷含量测量值约为0.46至0.81µg/g,为样品的95%置信水平和5次测量的平均值。根据参考文献对该方法进行了验证。用电化学方法和差分脉冲极谱(DPP)对实验结果进行了分析,结果一致。
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Investigation of Arsenic Content in Field Pesticides using inductively coupled plasma optical emission spectroscopy (ICP-OES)
In this study, Arsenic, which is found in the structure of field medicines, was determined by ICP-OES. For arsenic analysis, Turkey was elected four different commonly used pesticides. These pesticides were commercially named A, B, C, and D samples. These samples were solubilized using the appropriate procedure by microwave digestion method. For arsenic determination, 188.980 nm wavelength measurements were made. The determination of the known acid first with ICP-OES was measured at high sensitivity. Arsenic amounts were measured as approximately 0.46 to 0.81 µg/g as the 95% confidence level in the samples and the average of 5 measurements. The validation process of this method was done according to the reference article. The results of the experiment were made with the electrochemical method, differential pulse polarography (DPP), and the results were found to be in agreement.
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