用于连续微波辅助合成金属纳米颗粒的棱柱形施加器

P. Veronesi, R. Rosa, C. Leonelli, A. Cappi, A. Barzanti, G. Baldi
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引用次数: 1

摘要

金属(银、金、铜)纳米颗粒悬浮液在医学上的应用越来越受到关注。在现有的合成路线中,微波处理可以更好地控制粒度,实现产品的高纯度。纳米颗粒的大规模生产需要开发工业上可行的工艺,最好使用“绿色化学”方法,在环境压力和相对较低的温度下进行。基于最近开发的微波辅助水溶液处理工艺,设计了一种新型的专用连续流反应器,该反应器由两个双棱镜施加器组成,并进行了优化和测试。它可以生产高达1000升/天的金属纳米颗粒胶体悬浮液。
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Prismatic applicator for continuous microwave-assisted synthesis of metallic nanoparticles
Metallic (Ag, Au, Cu) nanoparticles suspensions are gaining an increasing interest in medical applications. Among the existing synthetic routes available, microwave processing allows to better control particle size and to achieve high purity of the products. The large scale production of nanoparticles requires the development of industrially-viable processes, preferably conducted using a “green chemistry” approach, at ambient pressure and relatively low temperature. Based on a recently developed microwave-assisted process in aqueous solution, a new dedicated continuous-flow reactor, made of two twin prismatic applicators has been designed, optimized and tested. It can produce up to 1000 liters/day of metal nanoparticles colloidal suspension.
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