热生成金纳米颗粒的原子力显微镜研究

A. Bonyár, Balazs Wimmer, I. Csarnovics
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引用次数: 2

摘要

将5 ~ 30 nm的金薄膜溅射在玻璃衬底上,通过热退火法制备了金纳米颗粒。通过改变热退火条件(温度和退火时间),制备出不同尺寸的纳米颗粒。利用原子力显微镜(AFM)对纳米颗粒的大小和分布进行了表征。金NP修饰表面拟用于表面等离子体共振成像(SPRi)仪器的传感器换能器元件。因此,我们研究了产生的NP信号的大小与退火参数的关系,以达到SPRi器件中NP信号放大的最佳条件。
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Investigation of thermally generated gold nanoparticles with AFM
Gold nanoparticles (Au NPs) were generated by thermally annealing gold thin films (5-30 nm) which were sputtered on glass substrates. The conditions of the thermal annealing (temperature and annealing time) were varied in order to generate nanoparticles in different sizes. The size and distribution of the nanoparticles were characterized by atomic force microscopy (AFM). The Au NP modified surface is intended to be used as sensor transducer element in a surface plasmon resonance imaging (SPRi) instrument. Thus we investigated the size of the generated NPs in function of the annealing parameters in order to reach optimal conditions for the NP signal amplification in the SPRi device.
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