马拉提亚椴树籽油不同溶剂提取及性质研究

Yunus Önal, Tuğçe Begüm Mumcu, Tuğba Utku
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摘要

本研究采用溶剂萃取法提取马拉提亚地区椴树籽油,并对其进行表征。2018年8月底,采集马拉提亚地区椴树种子,用索氏装置分离种子外壳,提取油脂。在索氏装置中,丙酮、己烷和乙醇作为溶剂。为了确定所得油的油质,对所得油进行了XRD、SEM、元素分析、灰分测定、皂化数等多项分析。结果表明,丙酮的收率为28%,己烷的收率为28.65%,乙醇的收率为33%。在菩提树种子的脂肪酸组成中,按重量计算的值为油酸:丙酮27,442,己烷30,852,棕榈酸:丙酮10,9545,己烷11,929,亚油酸:丙酮51188,己烷44145。在mg KOH/g油中己烷的皂值为176.72;丙酮为246.94;结果发现,乙醇为232.48。灰分测定值平均值为5575%;树皮灰分的差异为2.1%。
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Extraction and characterization of linden tree seed oil grown in Malatya with different solvents
In this study, the oil of linden seeds collected from Malatya region was taken by solvent extraction method and their characterization was made. Seeds for experiments at the end of August 2018, linden seeds in Malatya region were collected and their outer shells were separated from the seeds and oil was obtained with a Soxhlet device. Acetone, hexane and ethyl alcohol were used as solvents in the Soxhlet device. In order to determine the oil quality of the obtained oils, XRD, SEM, elemental analysis, ash determination, saponification number were subjected to a number of analyzes. As a result of the analyzes made, the oil yield with acetone was 28% by weight, with hexane 28.65% and 33% ethyl alcohol values were determined. In the fatty acid composition of linden tree seeds, the values by weight were found to be oleic acid: 27,442 for acetone, 30,852 for hexane, 10,9545 for palmitic acid: acetone, 11,929 for hexane, 51,188 for linoleic acid: acetone, 44,145 for hexane. The soap number values are 176.72 for hexane in mg KOH/g oil; 246.94 for acetone; It was found as 232.48 for ethyl alcohol. Ash determination values average 5,575%; bark ash was found to be 2.1% differently.
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