Ti-Al-C-N涂层沉积反应气体比对刀具耐磨性影响的研究

K. Ramazanov, E. Vardanyan, V. Mukhamadeev, A. Nazarov, I. Mukhamadeev, A. Nikolaev
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摘要

本文介绍了合成Ti-Al-C-N体系碳氮化物涂层时反应气体组分组成对刀具耐久性的影响。采用改进后的NNV-6.6-I1装置,在白炽阴极等离子体源的辅助下,从两个单组分阴极喷涂涂层。涂布时,将N2、氮气、C2H2、乙炔按1:4、2:3、3:2、4:1的比例混合反应气体送入腔室。本文介绍了所研究样品的显微硬度测量结果,结果表明,在N2:C2H2=2:3的反应气体比下沉积的涂层样品的显微硬度值最大(4870 HV0.05)。本文介绍了用所研究的涂层对硬质合金刀具进行现场试验的结果。耐久性测试表明,在氮气:C2H2=4:1的气体比下沉积涂层的刀具,与没有涂层的刀具相比,刀具耐久性提高了10倍。利用电子显微镜方法,对刀具切削面的化学成分进行了分析。对切割后表面的化学成分分析表明,以氮气与乙炔反应气体比例为4:1沉积的涂层样品表面的涂层元素含量明显高于其他涂层,表明涂层磨损较小。然而,铁存在于切削面的某些区域,这说明了处理过的材料与刀具的粘附性。
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The study of influence of the reaction gases ratio at the Ti–Al–C–N coating deposition on the cutting tool wear resistance
The paper presents the results of the study of the component composition of the reaction gases mixture when synthesizing carbonitride coatings of the Ti–Al–C–N system influencing the cutting tool durability. The coating was applied using the updated unit NNV-6.6-I1 by spraying from two one-component cathodes assisted by the incandescent cathode plasma source. During applying the coating, the mixture of reaction gases of N2 nitrogen and C2H2 acetylene in the ratio of 1:4, 2:3, 3:2, and 4:1 was delivered to the chamber. The paper presents the results of measuring the microhardness of studied specimens, which show that a sample with the coating deposited at the reaction gases ratio of N2:C2H2=2:3 had the largest microhardness value (4870 HV0.05). The paper presents the results of field tests of carbide-tipped tools with the studied coatings. Durability tests identified that a cutter with the coating deposited at the gas ratio of N2:C2H2=4:1 increases the tool durability ten times compared to a cutting tool without coating. Using the electron microscopy method, the authors investigated the chemical composition of the tool cutting face after tests. The analysis of the chemical composition of the surface after cutting showed that the content of coating elements on the surface of the sample with a coating deposited at the 4:1 ratio of the reaction gases of nitrogen and acetylene was considerably higher than that of other studied coatings, which indicates the less coating wear. However, ferrum is present in some areas of the cutting face, which says about the adhesion of treated material to the tool.
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