红外吸收光谱法鉴别盐酸甲基苯丙胺的研究

M. Amemiya, Y. Yanagisawa, T. Nagai
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引用次数: 0

摘要

用漫反射光谱法和透射光谱法对盐酸甲基苯丙胺的红外光谱进行了比较。前者的光谱在制备后保持不变,而后者则随着时间的推移而变化。漫反射光谱中常用的液样滴法在测定盐酸甲基苯丙胺红外光谱中简化了样品制备和纯化。因此,利用自动换样器的液样滴法进行反射光谱测量,可以方便、快速地获得许多样品的红外光谱。
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Studies on the Identification of Methamphetamine hydrochloride by Infrared Absorption Spectra Method
The infrared spectrum of methamphetamine hydrochloride by diffuse reflectance spectroscopy was compared with that by transmission spectroscopy. The former spectrum remained unchanged after preparation of a KBr disc, while the latter changed with the elapse of time.   The liquid sample drop method which is frequently used in diffuse reflectance spectroscopy simplified sample preparation, and purification in the measurement of the infrared spectrum of methamphetamine hydrochloride.   Consequently, reflectance spectroscopic measurement by the liquid sample drop method using an auto-sample-changer made it possible to obtain the infrared spectra of many samples easily and quickly.
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