用纳米团簇沉积技术制备核壳型磁性纳米颗粒

J. Bai, Jianping Wang
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引用次数: 0

摘要

采用纳米粒子沉积枪和在线共溅射技术在玻璃衬底上制备了核壳型Au@Fe/sub 65/Co/sub 35/纳米结构。利用透射电子显微镜(TEM)观察了纳米颗粒的结晶、织构和纳米结构,并利用振动样品磁强计测量了纳米颗粒的磁性能。透射电镜(TEM)明暗图像和衍射图显示,所有FeCo纳米颗粒均为单晶,取向随机。在室温下测得的磁滞回线平均直径约为23 nm,矫顽力约为60 Oe。金壳厚度约为1 ~ 2nm。
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Fabrication of core-shell type magnetic nanoparticles by a nanocluster deposition technique
Nanoparticle deposition gun and on-line co-sputtering technique was used to prepare core-shell type Au@Fe/sub 65/Co/sub 35/ nanostructures on glass substrates. The crystallization, texture and nanostructures were observed by using transmission electron microscopy (TEM), while the magnetic properties of the nanoparticles were measured by the use of a vibrating sample magnetometer. TEM observations including bright/dark images and diffraction patterns showed that all FeCo nanoparticles are single crystals and show random orientations. The hysteresis loop measured at room temperature has an average diameter of about 23 nm, and the coercivity is about 60 Oe. Au shell thickness is about 1-2 nm.
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