掺铁纳米TiO2的形态、元素、结构和光学性质研究

M. Ahmad, H. M. A. Javed, Asad Ali, Zaheer Ul Hassan, M. Afzaal, Muhammad Arif, S. Hussain
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引用次数: 0

摘要

在本研究中,采用溶胶-凝胶技术合成了fe掺杂的TiO2纳米颗粒,然后在真空中450℃退火。研究了fe掺杂对TiO2纳米粒子形态、元素、结构和光学性能的影响。用XRD分析了合成的纯TiO2纳米粒子和掺铁TiO2纳米粒子的结构性质。表面分析采用扫描电镜进行。用紫外/可见光谱法测定其光学性质。形貌分析表明,TiO2纳米颗粒呈球形。EDX分析证实了fe掺杂TiO2纳米颗粒的元素组成。XRD谱图表明,TiO2的衍射峰属于锐钛矿相。
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Investigation of Morphological, Elemental, Structural, and Optical Properties of Fe-Doped TiO2 Nanoparticles
In this research, Fe-doped TiO2 nanoparticles were synthesized by sol-gel technique followed by annealing at 450 oC in a vacuum. The effects of Fe-doping on the morphological, elemental, structural and optical properties of TiO2 nanoparticles have been investigated. XRD analysis was performed to examine the structural properties of synthesized pure TiO2 nanoparticles and Fe-doped TiO2 nanoparticles. Surface analysis was done using Scanning Electron Microscopy. Optical properties were determined using UV/Vis spectroscopy. Morphological analysis revealed that TiO2 nanoparticles have a spherical shape. EDX analysis confirmed the elemental composition of Fe-doped TiO2 nanoparticles. XRD patterns showed that diffraction peaks can be attributed to TiO2 with the anatase phase.
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