{"title":"用聚丙烯腈作显色剂的流动注射分光光度法测定钙","authors":"L. Jamil, S. A. Rahim","doi":"10.1109/ICOASE.2018.8548884","DOIUrl":null,"url":null,"abstract":"A spectrophotometric method for determination of Ca in aqueous solution using 1-(2-pyridylazo)-2-naphthol (PAN) as color reagent based on the formation of Ca-PAN Complex at pH 12 and measuring absorbance at 550nm, with molar absorptivity of 1.70×104 L.mol-1cm-1 has been modified to a flow injection-spectrophotometric (FI) method. The modified FI method is rapid, accurate, precise, and with low operation cost. The linear range of 1-8ppm was obtained with average recovery of 103.46 and precision of 1.5-3.4%. The proposed FI method using PAN as a color reagent was applied satisfactorily for the assay of Ca in natural water, milk, yogurt and human serum.","PeriodicalId":144020,"journal":{"name":"2018 International Conference on Advanced Science and Engineering (ICOASE)","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2018-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Flow-Injection Specrophotomemic Determination of Calcium Using PAN as a Color Agent\",\"authors\":\"L. Jamil, S. A. Rahim\",\"doi\":\"10.1109/ICOASE.2018.8548884\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A spectrophotometric method for determination of Ca in aqueous solution using 1-(2-pyridylazo)-2-naphthol (PAN) as color reagent based on the formation of Ca-PAN Complex at pH 12 and measuring absorbance at 550nm, with molar absorptivity of 1.70×104 L.mol-1cm-1 has been modified to a flow injection-spectrophotometric (FI) method. The modified FI method is rapid, accurate, precise, and with low operation cost. The linear range of 1-8ppm was obtained with average recovery of 103.46 and precision of 1.5-3.4%. The proposed FI method using PAN as a color reagent was applied satisfactorily for the assay of Ca in natural water, milk, yogurt and human serum.\",\"PeriodicalId\":144020,\"journal\":{\"name\":\"2018 International Conference on Advanced Science and Engineering (ICOASE)\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2018-10-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"2018 International Conference on Advanced Science and Engineering (ICOASE)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/ICOASE.2018.8548884\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"2018 International Conference on Advanced Science and Engineering (ICOASE)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/ICOASE.2018.8548884","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Flow-Injection Specrophotomemic Determination of Calcium Using PAN as a Color Agent
A spectrophotometric method for determination of Ca in aqueous solution using 1-(2-pyridylazo)-2-naphthol (PAN) as color reagent based on the formation of Ca-PAN Complex at pH 12 and measuring absorbance at 550nm, with molar absorptivity of 1.70×104 L.mol-1cm-1 has been modified to a flow injection-spectrophotometric (FI) method. The modified FI method is rapid, accurate, precise, and with low operation cost. The linear range of 1-8ppm was obtained with average recovery of 103.46 and precision of 1.5-3.4%. The proposed FI method using PAN as a color reagent was applied satisfactorily for the assay of Ca in natural water, milk, yogurt and human serum.
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