有机和非有机样品的μ-XRFA和μ-EXAFS测量:状态报告

A. Erko
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引用次数: 2

摘要

本文综述了BESSY的KMC-2光束线在空间分辨x射线测量中的微米和纳米分辨率的能力。讨论了微x射线荧光分析(μXRFA)、微扩展x射线吸收精细结构(μEXAFS)、微x射线吸收近边结构(μXANES)和驻波技术(SWT)作为同步辐射表征有机和非有机样品的有力方法的应用。采用单毛细和多毛细光学系统,通过μXRFA制图、μEXAFS和μXANES对有机和非有机样品进行了表征。介绍了在嵌入金波导结构的Si/W/Si三层中深度分辨钨XAFS测量的结果。已经实现了1nm量级的深度分辨率。
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μ-XRFA and μ-EXAFS measurements of organic and non-organic samples: status report
The capabilities of the KMC-2 beamline at BESSY for spatially resolved x-ray measurements with micro- and nanometer resolution are reviewed. An application of micro- X-ray fluorescence analysis (μXRFA), micro-extended X-ray absorption fine structure (μEXAFS), micro-X-ray absorption near-edge structure (μXANES) as well as standing wave technique (SWT) as a powerful method for the organic and non-organic samples characterization with synchrotron radiation is discussed. Mono and poly-capillary optical systems were used for characterization of organic and non-organic samples, by means of μXRFA mapping and μEXAFS and μXANES. The results of depth resolved tungsten XAFS measurements in a Si/W/Si trilayer embedded in a Au waveguide structure are presented. A depth resolution on the order of 1nm has been achieved.
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