L1/sub 0/ FePt薄膜晶粒尺寸的减小和有序温度

A. Sun, P. Kuo, J. Hsu, H.L. Huang
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引用次数: 3

摘要

本研究提出了一种降低L1/sub 0/ FePt薄膜有序温度的有效方法。这些薄膜的厚度从10 nm到200 nm不等,由传统磁控溅射系统在直流电源下制备,然后在真空中进行后镀。采用Cu-K/spl α /辐射x射线衍射(XRD)和透射电子显微镜(TEM)明场图像对膜的物相和微观结构进行了表征。TEM亮场图像显示膜的平均晶粒尺寸约为6 nm。XRD谱图表明,当退火温度为(T/sub /) /spl / 300/spl℃时,薄膜中不存在有序结构。在T/sub / /spl温度/ 350/spl度/C时,无序fcc FePt相转变为有序L1/sub 0/ FePt相。在本研究中,由于沉积速率高,薄膜中容易形成空位。在沉积过程中,一些额外的能量被引入到沉积膜中,从而降低了有序-无序能垒。
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Reduction of grain size and ordering temperature in L1/sub 0/ FePt thin films
In this research, a more effective procedure for reducing the ordering temperature of the L1/sub 0/ FePt thin films is proposed. These thin films, with thickness varying from 10 nm to 200 nm, are prepared by conventional magnetron sputtering system with a dc power supply and then postannealed in vacuum. The phases and microstructures of the films are characterized by X-ray diffraction (XRD) with Cu-K/spl alpha/ radiation and transmission electron microscopy (TEM) bright field image, respectively. TEM bright field images show that the films have average grain sizes of about 6 nm. XRD patterns show that there is no evidence that ordered structure exists in the film when annealing temperature (T/sub an/) /spl les/ 300/spl deg/C. For T/sub an/ /spl ges/ 350/spl deg/C, the disordered fcc FePt phase transforms into the ordered L1/sub 0/ FePt phase. Vacancies into the film are formed easily due to the high deposition rate process in this investigation. Some extra energy is introduced into the as-deposited film during deposition and reduced the order-disorder energy barrier.
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