尼罗罗非鱼鳞羟基磷灰石对常规和树脂改性玻璃离子水泥表面硬度的影响(体外研究)

A. Yudhit, K. Harahap, Sabrina Chairunnisa Nasution
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引用次数: 2

摘要

修复材料的表面硬度影响其耐磨性和寿命。羟基磷灰石的加入可以改善修复材料的力学性能。鱼鳞中含有碳酸钙,可用于合成羟基磷灰石。本研究的目的是通过掺入不同wt%的黑罗非鱼鱼鳞羟基磷灰石来评价传统和树脂改性玻璃离子水门石的表面硬度。以黑罗非鱼鱼鳞为原料,采用煅烧法制备了羟基磷灰石。采用常规和树脂改性玻璃离子水水泥制备直径为5mm、高度为2mm的样品,分为7组(n=10),分别为对照组、2wt% GIC、5wt% GIC、8wt% GIC、2wt% RMGIC、5wt% RMGIC和8wt% RMGIC。表面硬度用维氏硬度计测定。结果各组硬度值分别为49.81±3.55 VHN、34.49±1.82 VHN、32.58±1.61 VHN、36.63±3.09 VHN、32.05±3.77 VHN、36.23±4.27 VHN、19.27±1.71 VHN。单因素方差分析显示,各组间差异有统计学意义(p <0.05)。结果表明,鱼鳞羟基磷灰石对常规和树脂改性玻璃离子水泥的表面硬度有影响,而对常规GIC的硬度有降低作用,对RMGIC的硬度有提高作用。
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Effect of Hydroxyapatite From Nile Tilapia (Oreochromisniloticus) Scale on Surface Hardness of Conventional and Resin Modified Glass Ionomer Cement (In Vitro Study)
Surface hardness of restoration materials affected its wear resistance and longevity. The addition of hydroxyapatite could improve mechanical properties of restoration material. Hydroxyapatite can be synthesized from fish scales for it contain calcium carbonate. The aim of this study was to evaluate the surface hardness of conventional and resin modified glass ionomers cement by incorporation of different wt% of hydroxyapatite from Black tilapia (Oreochromisniloticus) scales. Hydroxyapatite was synthesized from black tilapia scales by calcination method. Samples with a diameter of 5 mm and a height of 2 mm were made from conventional and resin modified glass ionomer cement, then divided into 7 groups (n=10), namely control, 2wt% GIC, 5wt% GIC, 8wt% GIC, 2wt% RMGIC, 5wt% RMGIC, and 8wt% RMGIC. Surface hardness test was measured with Vickers Hardness Tester. Result showed hardness value from each groups respectively were 49.81 ± 3.55 VHN, 34.49 ± 1.82 VHN, 32.58 ± 1.61 VHN, 36.63 ± 3.09 VHN, 32.05 ± 3.77 VHN, 36.23 ± 4.27 VHN, and 19.27 ± 1.71 VHN. One-way ANOVA test showed a significant differences in all group (p <0.05). It can be conclude that hydroxyapatite from fish scale had an effect on surface hardness of conventional and resin modified glass ionomer cement, whereas it decreased the hardness of conventional GIC, yet it increased the RMGIC hardness.
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