{"title":"可3D打印柔性丙烯酸酯基树脂的制备与表征","authors":"Melinda Szalóki, Aaisha Akhtar Kabli, Csaba Hegedűs","doi":"10.33891/fsz.116.3.104-109","DOIUrl":null,"url":null,"abstract":"The aim of this study was to prepare an acrylate-based 3D printable resin that showed flexible properties after photopolymerizationand to characterize mechanical-physicochemical properties of polymerized objects. The experimental resincontained butyl acrylate (BA) and urethane dimethacrylate (UDMA) in 7:3 weight ratio, phenylbis(2,4,6-trimethylbenzoyl)phosphine oxide (BAPO) in 0.2 %w/w and ethyl 4-(dimethylamino) benzoate in 0.4 %w/w. Tensile strength measurementswere performed by Intron 5544. The curing times were 1, 2 and 5 min. FT-IR spectroscopy was used for the degreeof conversion (DC) measurements on the top and bottom surfaces of specimens. The tensile strength data of resinincreased with polymerization time. Behind this is a higher degree of polymerization, which is also supported by the conversiondata. A trial printing of experimental resin revealed that this matrix can be applied in an SLA 3D printer.","PeriodicalId":75851,"journal":{"name":"Fogorvosi szemle","volume":"31 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-09-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Preparation and characterization of 3D printable flexible acrylate-based resin\",\"authors\":\"Melinda Szalóki, Aaisha Akhtar Kabli, Csaba Hegedűs\",\"doi\":\"10.33891/fsz.116.3.104-109\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The aim of this study was to prepare an acrylate-based 3D printable resin that showed flexible properties after photopolymerizationand to characterize mechanical-physicochemical properties of polymerized objects. The experimental resincontained butyl acrylate (BA) and urethane dimethacrylate (UDMA) in 7:3 weight ratio, phenylbis(2,4,6-trimethylbenzoyl)phosphine oxide (BAPO) in 0.2 %w/w and ethyl 4-(dimethylamino) benzoate in 0.4 %w/w. Tensile strength measurementswere performed by Intron 5544. The curing times were 1, 2 and 5 min. FT-IR spectroscopy was used for the degreeof conversion (DC) measurements on the top and bottom surfaces of specimens. The tensile strength data of resinincreased with polymerization time. Behind this is a higher degree of polymerization, which is also supported by the conversiondata. A trial printing of experimental resin revealed that this matrix can be applied in an SLA 3D printer.\",\"PeriodicalId\":75851,\"journal\":{\"name\":\"Fogorvosi szemle\",\"volume\":\"31 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-09-14\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Fogorvosi szemle\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.33891/fsz.116.3.104-109\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Fogorvosi szemle","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.33891/fsz.116.3.104-109","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Preparation and characterization of 3D printable flexible acrylate-based resin
The aim of this study was to prepare an acrylate-based 3D printable resin that showed flexible properties after photopolymerizationand to characterize mechanical-physicochemical properties of polymerized objects. The experimental resincontained butyl acrylate (BA) and urethane dimethacrylate (UDMA) in 7:3 weight ratio, phenylbis(2,4,6-trimethylbenzoyl)phosphine oxide (BAPO) in 0.2 %w/w and ethyl 4-(dimethylamino) benzoate in 0.4 %w/w. Tensile strength measurementswere performed by Intron 5544. The curing times were 1, 2 and 5 min. FT-IR spectroscopy was used for the degreeof conversion (DC) measurements on the top and bottom surfaces of specimens. The tensile strength data of resinincreased with polymerization time. Behind this is a higher degree of polymerization, which is also supported by the conversiondata. A trial printing of experimental resin revealed that this matrix can be applied in an SLA 3D printer.