{"title":"高效液相色谱-质谱联用法测定花生基质中白藜芦醇的含量","authors":"Vidya Sagar Venkata Pasupuleti, Prashant Bagade, Naga Suresh Reddy Venkata Kachireddy","doi":"10.25303/2709rjce046052","DOIUrl":null,"url":null,"abstract":"A precise and very efficient tandem mass spectrometry method (LC-MS/MS) was developed to quantify the resveratrol in the peanut matrix. Two mobile phases made up of water and acetonitrile in a ratio of 98:2 (%v/v) with 0.1% formic acid and acetonitrile and water in a percentage of 98:2 %(v/v) with 0.1% formic acid were used in the LC-MS/MS analysis of resveratrol on a BEH C-18, 130A° (50mm 2.1mm, 1.7μm) analytical column with 0.3 mL/min of flow rate. A triple quadrupole mass spectrometer and a positive electrospray ionization system were used to quantify resveratrol in multiple reaction monitoring (MRM) modes. The technique was evaluated and was found capable of quantifying resveratrol in peanut samples starting at 10 ng/g in compliance with SANTE guidelines.","PeriodicalId":21012,"journal":{"name":"Research Journal of Chemistry and Environment","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2023-08-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"A Sensitive and High Throughput LC-MS/MS Method for the Determination of Resveratrol in Peanut Matrix\",\"authors\":\"Vidya Sagar Venkata Pasupuleti, Prashant Bagade, Naga Suresh Reddy Venkata Kachireddy\",\"doi\":\"10.25303/2709rjce046052\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A precise and very efficient tandem mass spectrometry method (LC-MS/MS) was developed to quantify the resveratrol in the peanut matrix. Two mobile phases made up of water and acetonitrile in a ratio of 98:2 (%v/v) with 0.1% formic acid and acetonitrile and water in a percentage of 98:2 %(v/v) with 0.1% formic acid were used in the LC-MS/MS analysis of resveratrol on a BEH C-18, 130A° (50mm 2.1mm, 1.7μm) analytical column with 0.3 mL/min of flow rate. A triple quadrupole mass spectrometer and a positive electrospray ionization system were used to quantify resveratrol in multiple reaction monitoring (MRM) modes. The technique was evaluated and was found capable of quantifying resveratrol in peanut samples starting at 10 ng/g in compliance with SANTE guidelines.\",\"PeriodicalId\":21012,\"journal\":{\"name\":\"Research Journal of Chemistry and Environment\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-08-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Research Journal of Chemistry and Environment\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.25303/2709rjce046052\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"Earth and Planetary Sciences\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Research Journal of Chemistry and Environment","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.25303/2709rjce046052","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"Earth and Planetary Sciences","Score":null,"Total":0}
A Sensitive and High Throughput LC-MS/MS Method for the Determination of Resveratrol in Peanut Matrix
A precise and very efficient tandem mass spectrometry method (LC-MS/MS) was developed to quantify the resveratrol in the peanut matrix. Two mobile phases made up of water and acetonitrile in a ratio of 98:2 (%v/v) with 0.1% formic acid and acetonitrile and water in a percentage of 98:2 %(v/v) with 0.1% formic acid were used in the LC-MS/MS analysis of resveratrol on a BEH C-18, 130A° (50mm 2.1mm, 1.7μm) analytical column with 0.3 mL/min of flow rate. A triple quadrupole mass spectrometer and a positive electrospray ionization system were used to quantify resveratrol in multiple reaction monitoring (MRM) modes. The technique was evaluated and was found capable of quantifying resveratrol in peanut samples starting at 10 ng/g in compliance with SANTE guidelines.
京公网安备 11010802042870号
京ICP备2023020795号-1
分享
求助内容：
应助结果提醒方式：
扫码关注我们
