Subramanian Mohanaparameswari, Manavalan Balachandramohan, Ponnusamy Sasikumar, Chinnaiyan Rajeevgandhi, Mark Vimalan, Sanmugam Pugazhendhi, Krishnamurthy Ganesh Kumar, Salim Albukhaty, Ghassan M. Sulaiman, Mosleh M. Abomughaid, Mohammed Abu-Alghayth
{"title":"绿色合成法研究龙葵/薄荷叶提取物AgO纳米颗粒的结构性质及抗菌活性","authors":"Subramanian Mohanaparameswari, Manavalan Balachandramohan, Ponnusamy Sasikumar, Chinnaiyan Rajeevgandhi, Mark Vimalan, Sanmugam Pugazhendhi, Krishnamurthy Ganesh Kumar, Salim Albukhaty, Ghassan M. Sulaiman, Mosleh M. Abomughaid, Mohammed Abu-Alghayth","doi":"10.1515/gps-2023-0080","DOIUrl":null,"url":null,"abstract":"Abstract Solanum nigrum and Mentha leaf extracts were used as reducing and stabilizing reagents in the green synthesis of silver oxide nanoparticles (AgO NPs), and their antibacterial efficacy was subsequently evaluated. The structure and morphology of AgO NPs were evaluated using X-ray diffraction and filed emission scanning electron microscope. High-resolution transmission electron microscopy images were used to analyze the characteristics of certain particles with clearly discernible atomic structures. The functional group and elemental composition of AgO NPs were investigated using fourier transform infrared spectroscopy and energy dispersive X-ray spectroscopy. Ultraviolet–visible spectroscopy was used to determine the energy band gap ( E g ) of the sample. The dielectric constant of both samples was found to be inversely proportional to frequency, whereas the dielectric loss was found to be directly proportional to temperature but directly proportional to frequency. This suggests that the space charge has an effect on the mechanism of charge transfer as well as polarizability. AC conductivity rises and is inversely proportional to temperature increases. AgO NPs had a size range of around 56 nm and were mostly spherical. The antibacterial potential of the synthesized AgO NPs using both extracts was compared by the well-diffusion method. AgO NPs at 50–100 µg·mL −1 concentration significantly inhibited the bacterial growth of Bacillus cereus , Staphylococcus aureus , Escherichia coli , and Klebsiella pneumonia .","PeriodicalId":12758,"journal":{"name":"Green Processing and Synthesis","volume":"21 1","pages":"0"},"PeriodicalIF":3.8000,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Investigation of structural properties and antibacterial activity of AgO nanoparticle extract from <i>Solanum nigrum/Mentha</i> leaf extracts by green synthesis method\",\"authors\":\"Subramanian Mohanaparameswari, Manavalan Balachandramohan, Ponnusamy Sasikumar, Chinnaiyan Rajeevgandhi, Mark Vimalan, Sanmugam Pugazhendhi, Krishnamurthy Ganesh Kumar, Salim Albukhaty, Ghassan M. Sulaiman, Mosleh M. Abomughaid, Mohammed Abu-Alghayth\",\"doi\":\"10.1515/gps-2023-0080\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Abstract Solanum nigrum and Mentha leaf extracts were used as reducing and stabilizing reagents in the green synthesis of silver oxide nanoparticles (AgO NPs), and their antibacterial efficacy was subsequently evaluated. The structure and morphology of AgO NPs were evaluated using X-ray diffraction and filed emission scanning electron microscope. High-resolution transmission electron microscopy images were used to analyze the characteristics of certain particles with clearly discernible atomic structures. The functional group and elemental composition of AgO NPs were investigated using fourier transform infrared spectroscopy and energy dispersive X-ray spectroscopy. Ultraviolet–visible spectroscopy was used to determine the energy band gap ( E g ) of the sample. The dielectric constant of both samples was found to be inversely proportional to frequency, whereas the dielectric loss was found to be directly proportional to temperature but directly proportional to frequency. This suggests that the space charge has an effect on the mechanism of charge transfer as well as polarizability. AC conductivity rises and is inversely proportional to temperature increases. AgO NPs had a size range of around 56 nm and were mostly spherical. The antibacterial potential of the synthesized AgO NPs using both extracts was compared by the well-diffusion method. AgO NPs at 50–100 µg·mL −1 concentration significantly inhibited the bacterial growth of Bacillus cereus , Staphylococcus aureus , Escherichia coli , and Klebsiella pneumonia .\",\"PeriodicalId\":12758,\"journal\":{\"name\":\"Green Processing and Synthesis\",\"volume\":\"21 1\",\"pages\":\"0\"},\"PeriodicalIF\":3.8000,\"publicationDate\":\"2023-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Green Processing and Synthesis\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1515/gps-2023-0080\",\"RegionNum\":4,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"CHEMISTRY, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Green Processing and Synthesis","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1515/gps-2023-0080","RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
Investigation of structural properties and antibacterial activity of AgO nanoparticle extract from Solanum nigrum/Mentha leaf extracts by green synthesis method
Abstract Solanum nigrum and Mentha leaf extracts were used as reducing and stabilizing reagents in the green synthesis of silver oxide nanoparticles (AgO NPs), and their antibacterial efficacy was subsequently evaluated. The structure and morphology of AgO NPs were evaluated using X-ray diffraction and filed emission scanning electron microscope. High-resolution transmission electron microscopy images were used to analyze the characteristics of certain particles with clearly discernible atomic structures. The functional group and elemental composition of AgO NPs were investigated using fourier transform infrared spectroscopy and energy dispersive X-ray spectroscopy. Ultraviolet–visible spectroscopy was used to determine the energy band gap ( E g ) of the sample. The dielectric constant of both samples was found to be inversely proportional to frequency, whereas the dielectric loss was found to be directly proportional to temperature but directly proportional to frequency. This suggests that the space charge has an effect on the mechanism of charge transfer as well as polarizability. AC conductivity rises and is inversely proportional to temperature increases. AgO NPs had a size range of around 56 nm and were mostly spherical. The antibacterial potential of the synthesized AgO NPs using both extracts was compared by the well-diffusion method. AgO NPs at 50–100 µg·mL −1 concentration significantly inhibited the bacterial growth of Bacillus cereus , Staphylococcus aureus , Escherichia coli , and Klebsiella pneumonia .
期刊介绍:
Green Processing and Synthesis is a bimonthly, peer-reviewed journal that provides up-to-date research both on fundamental as well as applied aspects of innovative green process development and chemical synthesis, giving an appropriate share to industrial views. The contributions are cutting edge, high-impact, authoritative, and provide both pros and cons of potential technologies. Green Processing and Synthesis provides a platform for scientists and engineers, especially chemists and chemical engineers, but is also open for interdisciplinary research from other areas such as physics, materials science, or catalysis.