低温等离子体绿色合成KO纳米颗粒及其抗菌性能研究

Q2 Pharmacology, Toxicology and Pharmaceutics Science and Technology Indonesia Pub Date : 2023-10-01 DOI:10.26554/sti.2023.8.4.579-584
Mohammed Jawad Kadhim, Rana Ismael Khaleel, Karar Mahdi Talib, Raghad S. Mohammed
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引用次数: 0

摘要

采用冷等离子体技术,以玫瑰叶提取物为原料,以氯化钾(KCl)为原料合成氧化钾纳米颗粒(KO NPs),并对其物理和生物学特性进行了研究。采用扫描电子显微镜(SEM)、x射线衍射仪(XRD)、x射线色散光谱(EDS)和紫外可见光谱(UV-Vis)对KO纳米颗粒的物理性质进行了表征。XRD分析表明,KO NPs的平均晶粒尺寸为108 nm。EDX分析表明形成了高纯度的KO NPs。SEM图像显示了一些KO NPs的球形形状,大小从44.66 nm到134 nm不等。根据KO纳米粒子的紫外可见光谱,这些纳米粒子的吸收边缘呈现蓝移,能隙范围(Eg)在2.8 ~ 3.4 eV之间。并通过抗菌和抗真菌活性检测了KO NPs的生物学功效。为了评价KO NPs的体外毒性,我们对其进行了体外抑菌试验。对部分受试菌,KO NPs表现出良好的抗菌活性。
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Green Synthesis of KO Nanoparticles by Cold Plasma and Study of Their Properties for Antibacterial Applications
This study used the cold plasma technique to synthesize potassium oxide nanoparticles (KO NPs) from potassium chloride (KCl) with roselle extract leaves and examine their physical and biological characterization. The physical properties of KO nanoparticles were examined by Scanning Electron Microscopy (SEM), X-Ray Diffraction (XRD), X-Ray Dispersive Spectroscopy (EDS), and UV–Vis Spectroscopy. Analyses of XRD show the KO NPs with an average crystallite size of 108 nm. The EDX analysis shows that high-purity KO NPs have formed. SEM image shows the shapes of some KO NPs’ spherical with varying sizes ranging from 44.66 nm to 134 nm. According to UV–Vis spectra of KO NPs, the absorption edge of these nanoparticles exhibited a blueshift with an energy gap range (Eg) from 2.8 to 3.4 eV. The biological efficacy of KO NPs was also examined by testing their antibacterial and antifungal activity. To evaluate the toxicity of the KO NPs were tested in vitro and activated as antibacterial. Against some of the test organisms, the KO NPs demonstrated good antibacterial activity.
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来源期刊
Science and Technology Indonesia
Science and Technology Indonesia Pharmacology, Toxicology and Pharmaceutics-Pharmacology, Toxicology and Pharmaceutics (miscellaneous)
CiteScore
1.80
自引率
0.00%
发文量
72
审稿时长
8 weeks
期刊最新文献
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