溶胶-凝胶法制备蔗渣纳米二氧化硅

Nano particle Pub Date : 2023-02-16 DOI:10.35702/nano.10010
Yatim Lailun Ni’mah, Zakkiyyah Hidayatul Muhaiminah, Suprapto Suprapto
{"title":"溶胶-凝胶法制备蔗渣纳米二氧化硅","authors":"Yatim Lailun Ni’mah, Zakkiyyah Hidayatul Muhaiminah, Suprapto Suprapto","doi":"10.35702/nano.10010","DOIUrl":null,"url":null,"abstract":"The silica nanoparticles have been successfully synthesized from sugarcane bagasse using the sol-gel method. Sugarcane bagasse contains abundant silica, so it can use as an alternative source of silica nanoparticles. Sugarcane bagasse was calcined at 650°C for 2 hours, and then it was extracted using NaOH to obtain sodium silicate solution. The solution was titrated with HCl for gelling process. The synthesized of silica nanoparticles from sugarcane bagasse were characterized using FTIR and XRD. Based on the XRD characterization, the results showed that the silica had an amorphous phase, and the FTIR spectrum has siloxane and silanol groups. The synthesized silica nanoparticles have an average size of 53 nm which was calculated using Scherrer Formula. From the data obtained, sugarcane bagasse can use as a source of silica nanoparticles.","PeriodicalId":478124,"journal":{"name":"Nano particle","volume":"232 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-02-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Synthesis of Silica Nanoparticles from Sugarcane Bagasse by Sol-Gel Method\",\"authors\":\"Yatim Lailun Ni’mah, Zakkiyyah Hidayatul Muhaiminah, Suprapto Suprapto\",\"doi\":\"10.35702/nano.10010\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The silica nanoparticles have been successfully synthesized from sugarcane bagasse using the sol-gel method. Sugarcane bagasse contains abundant silica, so it can use as an alternative source of silica nanoparticles. Sugarcane bagasse was calcined at 650°C for 2 hours, and then it was extracted using NaOH to obtain sodium silicate solution. The solution was titrated with HCl for gelling process. The synthesized of silica nanoparticles from sugarcane bagasse were characterized using FTIR and XRD. Based on the XRD characterization, the results showed that the silica had an amorphous phase, and the FTIR spectrum has siloxane and silanol groups. The synthesized silica nanoparticles have an average size of 53 nm which was calculated using Scherrer Formula. From the data obtained, sugarcane bagasse can use as a source of silica nanoparticles.\",\"PeriodicalId\":478124,\"journal\":{\"name\":\"Nano particle\",\"volume\":\"232 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-02-16\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Nano particle\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.35702/nano.10010\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Nano particle","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.35702/nano.10010","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1

摘要

以甘蔗渣为原料,采用溶胶-凝胶法制备了二氧化硅纳米颗粒。甘蔗渣中含有丰富的二氧化硅,因此可以作为二氧化硅纳米颗粒的替代来源。将甘蔗渣在650℃下煅烧2小时,然后用NaOH萃取得到水玻璃溶液。用盐酸滴定溶液进行胶凝过程。采用红外光谱(FTIR)和x射线衍射(XRD)对蔗渣合成的纳米二氧化硅进行了表征。XRD表征结果表明,二氧化硅具有非晶相,FTIR光谱具有硅氧烷和硅醇基团。合成的二氧化硅纳米颗粒的平均尺寸为53 nm,用Scherrer公式计算得到。从获得的数据来看,甘蔗渣可以作为二氧化硅纳米颗粒的来源。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Synthesis of Silica Nanoparticles from Sugarcane Bagasse by Sol-Gel Method
The silica nanoparticles have been successfully synthesized from sugarcane bagasse using the sol-gel method. Sugarcane bagasse contains abundant silica, so it can use as an alternative source of silica nanoparticles. Sugarcane bagasse was calcined at 650°C for 2 hours, and then it was extracted using NaOH to obtain sodium silicate solution. The solution was titrated with HCl for gelling process. The synthesized of silica nanoparticles from sugarcane bagasse were characterized using FTIR and XRD. Based on the XRD characterization, the results showed that the silica had an amorphous phase, and the FTIR spectrum has siloxane and silanol groups. The synthesized silica nanoparticles have an average size of 53 nm which was calculated using Scherrer Formula. From the data obtained, sugarcane bagasse can use as a source of silica nanoparticles.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Synthesis of Silica Nanoparticles from Sugarcane Bagasse by Sol-Gel Method
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1