优化玻璃纤维增强聚丙烯长纤维热塑性球团的热塑性拉挤参数

IF 2.1 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Polymers & Polymer Composites Pub Date : 2023-10-12 DOI:10.1177/09673911231207297
Ponlapath Tipboonsri, Anin Memon
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引用次数: 0

摘要

长纤维热塑性球团(LFTP)是一种包含热塑性增强的不连续纤维的球团。在本实验中,采用热塑性拉挤工艺生产lfp。该热塑性拉挤工艺在机器装置上简单,可提高LFTP的浸渍质量。增强纤维采用玻璃纤维,基体采用PP纤维。研究了成型温度和拉拔速度对浸渍的影响。模具系统包含六个加热区。在第一步中,3区和4区(熔化区)在200、210、220和230℃时变化。选择效果较好的熔化区进行下一步的研究。在第二步中,5区和6区(热还原区)分别在160°C - 190°C和150°C - 180°C变化。在确定最佳成型温度后,研究了拉拔速度,拉拔速度分别为10、20、30、40和50 cm/min。通过显微组织分析研究了LFTP的浸渍质量。用数据记录仪记录了拉挤模内的温度分布。并对热塑性拉挤法制备的LFTP的浸渍质量和微观结构进行了比较。结果表明,随着熔区温度的升高,未浸渍率降低。在热还原区,未浸渍率随温度的降低而降低。对于拉拔速度,未浸渍率随拉拔速度的降低而降低。优化后的模具系统的熔化区温度为230℃,热还原区温度为160℃和150℃。最佳拉拔速度为10 cm/min,未浸渍率为8.06%。商用LFTP的未浸渍率为13.73%。
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Optimizing thermoplastic pultrusion parameters for quality long fiber thermoplastic pellets in glass fiber-reinforced polypropylene
A long fiber thermoplastic pellet (LFTP) is a pellet that contains discontinuous fibers reinforced in thermoplastic. In this experiment, LFTPs were produced using the thermoplastic pultrusion process. The thermoplastic pultrusion process is uncomplicated in terms of the machine device, and it can improve the impregnation quality of LFTP. Glass fiber was used as the reinforced fiber, and PP fiber was used as the matrix. This experiment studied the effect of molding temperature and pulling speed on impregnation. The die system contained six heating zones. In the first step, zones 3 and 4 (melting zone) were varied at 200, 210, 220, and 230°C. The melting zone that exhibited good results was selected for the next step. In the second step, zones 5 and 6 (heat reduction zone) were varied at 160°C–190°C and 150°C–180°C, respectively. After determining the optimal molding temperature, the pulling speed was studied, with speeds varied at 10, 20, 30, 40, and 50 cm/min. The impregnated quality of the LFTP was investigated through microstructure analysis. A data logger was used to record the temperature profile in the pultrusion die. Furthermore, the impregnation quality and microstructure of LFTP from thermoplastic pultrusion were compared to commercial LFTP. The results showed that un-impregnation decreased with an increase in the melting zone temperature. In the heat reduction zone, un-impregnation decreased with a decrease in temperature. For the pulling speed, un-impregnation decreased with a decrease in speed. The optimal die system had a melting zone temperature of 230°C and a heat reduction zone temperature of 160 and 150°C. The optimal pulling speed was 10 cm/min, resulting in an un-impregnation rate of 8.06%. Additionally, commercial LFTP had an un-impregnation rate of 13.73%.
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来源期刊
Polymers & Polymer Composites
Polymers & Polymer Composites 工程技术-材料科学:表征与测试
CiteScore
4.30
自引率
9.50%
发文量
90
审稿时长
5.7 months
期刊介绍: Polymers & Polymer Composites provides a forum for the publication of expertly peer reviewed, international research into the following topics: - Fibre reinforced and particulate filled plastics - Engineering plastics - Nanocomposites - Polymers or polyblends intended for engineering use (including structural, load bearing electronic and electrical applications) - Fibre reinforced and particulate filled plastics - Structural adhesives - Textile & wood fibres - Biomaterials with a load bearing capacity, (including polymer based dental materials)
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