沉积的VT20和VT1-0合金样品过渡区化学元素的结构与分布

IF 0.9 4区 材料科学 Q3 MATERIALS SCIENCE, CERAMICS Powder Metallurgy and Metal Ceramics Pub Date : 2023-11-17 DOI:10.1007/s11106-023-00383-4
A. A. Skrebtsov, O. S. Omelchenko, J. I. Kononenko, A. M. Kaplunovska
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摘要

累积(或增材制造)工艺使部件的生产能够使各个部分具有适合其特定用途的不同化学成分。然而,熔合区内元素的分布及其大小仍未得到充分的了解。将VT1-0和VT20钛合金样品熔接,一种情况下将VT1-0合金粉末沉积在VT20铸造合金上,另一种情况下将VT20钛合金粉末沉积在VT1-0铸造合金上。无论粉末的粒度和化学成分如何,样品的化学成分均符合合金的相关标准。采用Neophot 32光学显微镜对其宏观结构进行研究。在所有沉积选项中,样品的孔隙度都最小。显微组织分析表明,沉积材料在纵向和横向上均呈均匀结构。具有特定化学成分的区域的显微组织与相关铸态合金相似。在粉末/铸造金属熔合线上观察到结构部件尺寸和形状的变化。在不同化学成分的钛合金熔合过程中发现了明显的过渡区。用扫描电镜观察了粉末/铸造金属熔合区纵、横截面的化学成分。在离熔合线不同距离处确定了化学成分。结果表明:化学元素重新分布,含量发生变化。通过显微结构研究确定了化学成分发生改变的区域的存在。对化学元素的分布进行了定性评价,发现其分布是均匀的。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Structure and Distribution of Chemical Elements in the Transition Zone in Deposited VT20 and VT1-0 Alloy Samples

Buildup (or additive manufacturing) processes enable the production of components where individual sections can possess distinct chemical compositions tailored to their specific purpose. However, the distribution of elements in the fusion zone and its sizes remain inadequately understood. Samples of VT1-0 and VT20 titanium alloys were fused so that the VT1-0 alloy powder was deposited onto the VT20 cast alloy in one case and the VT20 titanium alloy powder was deposited onto the VT1-0 cast alloy in the other. Regardless of the grain-size and chemical compositions of the powders, the chemical composition of the samples met relevant standards for the alloys. The macrostructures were studied employing a Neophot 32 optical microscope. Minimal porosity was revealed in the samples across all deposition options. Microstructural analysis showed that the deposited material formed a uniform structure both longitudinally and transversely. The microstructure in zones with specific chemical compositions resembled that of the associated as-cast alloys. Variations in the sizes and shapes of structural components were observed toward the powder/cast metal fusion line. A distinct transition zone was found in the fusion of titanium alloys with different chemical compositions. The chemical composition in the longitudinal and transverse sections in the powder/cast metal fusion zone was examined with a scanning electron microscope. The chemical composition was established at different distances from the fusion line. The results showed that the chemical elements redistributed and their contents changed. The presence of zones with altered chemical composition was ascertained by microstructural studies. The distribution of chemical elements was qualitatively assessed and found to be uniform.

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来源期刊
Powder Metallurgy and Metal Ceramics
Powder Metallurgy and Metal Ceramics 工程技术-材料科学:硅酸盐
CiteScore
1.90
自引率
20.00%
发文量
43
审稿时长
6-12 weeks
期刊介绍: Powder Metallurgy and Metal Ceramics covers topics of the theory, manufacturing technology, and properties of powder; technology of forming processes; the technology of sintering, heat treatment, and thermo-chemical treatment; properties of sintered materials; and testing methods.
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