由乙酰葡萄醌衍生的新型噻嗪醌类化合物的简易合成

IF 2.1 3区化学 Q3 CHEMISTRY, MULTIDISCIPLINARY Journal of Sulfur Chemistry Pub Date : 2024-03-03 DOI:10.1080/17415993.2023.2281595

Ashraf A. Aly , Kamal U. Sadek , Mohammed B. Alshammari , Akil Ahmad , Eman A. Aziz , Alan B. Brown , Asmaa H. Mohamed

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引用次数: 0

摘要

以氧苊-肼为原料，合成了2-氧苊-1(2H)-乙基肼-乙基肼)-5,6-二苯基-1,3-噻嗪-4-酮。

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Facile synthesis of new thiazinanones derived by acenaphythylenone

In an attempt to develop new thiazinanones, 2-oxoacenaphthylen-1(2H)-ylidene)hydrazineylidene)-5,6-diphenyl-1,3-thiazinan-4-ones were synthesized via the reaction of oxoacenaphthylen-hydrazinecarbothioamide derivatives with 2,3-diphenylcycloprop-2-enone in ethanol and catalyzed by triethyl amine. The structure of the obtained thiazinanones was elucidated by spectral data (IR, MS, ¹H and ¹³C NMR spectra) in addition to elemental analysis. The mechanism describes the reaction pathway was also discussed.

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来源期刊

Journal of Sulfur Chemistry CHEMISTRY, MULTIDISCIPLINARY-

CiteScore

4.10

自引率

9.10%

发文量

审稿时长

6-12 weeks

期刊介绍： The Journal of Sulfur Chemistry is an international journal for the dissemination of scientific results in the rapidly expanding realm of sulfur chemistry. The journal publishes high quality reviews, full papers and communications in the following areas: organic and inorganic chemistry, industrial chemistry, materials and polymer chemistry, biological chemistry and interdisciplinary studies directly related to sulfur science. Papers outlining theoretical, physical, mechanistic or synthetic studies pertaining to sulfur chemistry are welcome. Hence the target audience is made up of academic and industrial chemists with peripheral or focused interests in sulfur chemistry. Manuscripts that truly define the aims of the journal include, but are not limited to, those that offer: a) innovative use of sulfur reagents; b) new synthetic approaches to sulfur-containing biomolecules, materials or organic and organometallic compounds; c) theoretical and physical studies that facilitate the understanding of sulfur structure, bonding or reactivity; d) catalytic, selective, synthetically useful or noteworthy transformations of sulfur containing molecules; e) industrial applications of sulfur chemistry; f) unique sulfur atom or molecule involvement in interfacial phenomena; g) descriptions of solid phase or combinatorial methods involving sulfur containing substrates. Submissions pertaining to related atoms such as selenium and tellurium are also welcome. Articles offering routine heterocycle formation through established reactions of sulfur containing substrates are outside the scope of the journal.