添加剂 h-BN 对 Al2TiO5 复合物物理和机械性能的影响

IF 0.2 Q4 MULTIDISCIPLINARY SCIENCES Suranaree Journal of Science and Technology Pub Date : 2023-12-14 DOI:10.55766/sujst-2023-05-e02854
Paramapat Treetornkeerati, Montree Hankoy, M. Kitiwan, Mana Rodchom, S. Vichaphund, D. Atong, P. Tunthawiroon
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引用次数: 0

摘要

钛酸铝(Al2TiO5)具有热膨胀率低、熔点高和优异的耐腐蚀性等特点,是一种很有前途的高温应用材料。本研究探讨了添加 h-BN 对 Al2TiO5 复合材料性能的影响。复合材料是通过烧结摩尔比为 1:1 的 Al2O3 和 TiO2 混合物制备的,混合物中添加了不同量的 h-BN(5-20 摩尔%)。样品在 1,500ºC 的氮气环境中烧结 4 小时,并对复合材料的体积密度、孔隙率、相变、微观结构、抗弯强度和硬度进行了研究。XRD 分析证实了复合材料中存在 Al2TiO5、Al2O3 和 Al18B4O33 相。h-BN 的添加量从 5 mol% 增加到 20 mol%,使 Al2TiO5 复合材料的体积密度、抗弯强度和硬度逐渐提高。h-BN 含量最高(20 摩尔%)的复合材料的体积密度为 3.12 g/cm3,弯曲强度和硬度值也最高,分别为 123.6±8.9 MPa 和 11.2±4.1 GPa。
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EFFECT OF h-BN AS AN ADDITIVE ON PHYSICAL AND MECHANICAL PROPERTIES OF Al2TiO5 COMPOSITE
Aluminum titanate (Al2TiO5) is a promising material for high-temperature applications due to its low thermal expansion, high melting point, and excellent corrosion resistance. In this study, the effect of h-BN addition on the properties of Al2TiO5 composites was investigated. The composites were prepared by sintering a mixture of Al2O3 and TiO2 at a 1:1 molar ratio, with varying amounts of h-BN (5-20 mol%) added to the mixture. The samples were sintered at 1,500ºC for 4 h in an N2 atmosphere, and the bulk density, porosity, phase transition, microstructure, flexural strength, and hardness of the composites were investigated. XRD analysis confirmed the presence of Al2TiO5, Al2O3, and Al18B4O33 phases in the composites. The addition of h-BN in increasing amounts from 5 to 20 mol% resulted in a gradual improvement in the bulk density, flexural strength, and hardness of the Al2TiO5 composites. The composite with the highest h-BN content (20 mol%) exhibited a bulk density of 3.12 g/cm3, as well as the highest flexural strength and hardness values of 123.6±8.9 MPa and 11.2±4.1 GPa, respectively.
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来源期刊
Suranaree Journal of Science and Technology
Suranaree Journal of Science and Technology MULTIDISCIPLINARY SCIENCES-
CiteScore
0.30
自引率
50.00%
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0
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