基于交叉相关分析的 EBSD 探测器的世代评估:从闪烁体到直接探测

IF 2.1 3区 工程技术 Q2 MICROSCOPY Ultramicroscopy Pub Date : 2023-12-21 DOI:10.1016/j.ultramic.2023.113913
Josephine DeRonja , Matthew Nowell , Stuart Wright , Josh Kacher
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引用次数: 0

摘要

基于交叉相关的电子反向散射衍射技术于十多年前问世,可以在高空间分辨率下对晶体旋转和弹性应变梯度进行高精度测量。从那时起,电子探测器技术有了显著的进步,包括超高速探测器的出现和直接探测器的商业化。在本研究中,我们以单晶硅样品为基准,评估了多代电子探测器在基于交叉相关分析中的功效。我们的研究表明,虽然在精度方面的改进不大,但在高质量衍射图样的采集速度方面却有显著提高。这对可收集的数据集的大小具有重要影响,并可减少漂移和样品污染的影响。
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Generational assessment of EBSD detectors for cross-correlation-based analysis: From scintillators to direct detection

Introduced over ten years ago, cross-correlation-based electron backscatter diffraction has enabled high precision measurements of crystallographic rotations and elastic strain gradients at high spatial resolution. Since that time, there have been remarkable improvements in electron detector technology, including the advent of ultra-high speed detectors and the commercialization of direct detectors. In this study, we assess the efficacy of multiple generations of electron detectors for cross-correlation-based analysis using a single crystal Si sample as a reference. We show that, while improvements in precision are modest, there have been significant gains in the rate at which high-quality diffraction patterns can be collected. This has important implications in the size of datasets that can be collected and reduces the impact of drift and sample contamination.

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来源期刊
Ultramicroscopy
Ultramicroscopy 工程技术-显微镜技术
CiteScore
4.60
自引率
13.60%
发文量
117
审稿时长
5.3 months
期刊介绍: Ultramicroscopy is an established journal that provides a forum for the publication of original research papers, invited reviews and rapid communications. The scope of Ultramicroscopy is to describe advances in instrumentation, methods and theory related to all modes of microscopical imaging, diffraction and spectroscopy in the life and physical sciences.
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