用于药物分析的分散液-液微萃取技术的最新进展。

IF 4.2 2区 化学 Q1 CHEMISTRY, ANALYTICAL Critical reviews in analytical chemistry Pub Date : 2024-01-02 DOI:10.1080/10408347.2023.2299280
Karen Sze Jie Tay, Hong Heng See
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引用次数: 0

摘要

样品净化和预浓缩是药物分析的关键组成部分。分散液-液微萃取(DLLME)技术被公认为是提高整体检测灵敏度的最有效方法。虽然各种 DLLME 模式已在药物分析中得到了推广,但仍需更多地讨论专为这一领域开发的预浓缩技术。本综述全面概述了 2017 年至 2023 年 5 月期间用于药物分析的各种 DLLME 模式。综述涵盖了 DLLME 的原理、影响微萃取的因素、不同 DLLME 模式的选定应用及其优缺点。此外,报告还重点介绍了药物分析中采用的多重萃取策略。
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Recent Advances in Dispersive Liquid-Liquid Microextraction for Pharmaceutical Analysis.

Sample clean-up and pre-concentration are critical components of pharmaceutical analysis. The dispersive liquid-liquid microextraction (DLLME) technique is widely recognized as the most effective approach for enhancing overall detection sensitivity. While various DLLME modes have been advanced in pharmaceutical analysis, there need to be more discussions on pre-concentration techniques specifically developed for this field. This review presents a comprehensive overview of the different DLLME modes used in pharmaceutical analysis from 2017 to May 2023. The review covers the principles of DLLME, the factors affecting microextraction, the selected applications of different DLLME modes, and their advantages and disadvantages. Additionally, it focuses on multi-extraction strategies employed for pharmaceutical analysis.

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来源期刊
CiteScore
12.00
自引率
4.00%
发文量
137
审稿时长
6 months
期刊介绍: Critical Reviews in Analytical Chemistry continues to be a dependable resource for both the expert and the student by providing in-depth, scholarly, insightful reviews of important topics within the discipline of analytical chemistry and related measurement sciences. The journal exclusively publishes review articles that illuminate the underlying science, that evaluate the field''s status by putting recent developments into proper perspective and context, and that speculate on possible future developments. A limited number of articles are of a "tutorial" format written by experts for scientists seeking introduction or clarification in a new area. This journal serves as a forum for linking various underlying components in broad and interdisciplinary means, while maintaining balance between applied and fundamental research. Topics we are interested in receiving reviews on are the following: · chemical analysis; · instrumentation; · chemometrics; · analytical biochemistry; · medicinal analysis; · forensics; · environmental sciences; · applied physics; · and material science.
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