一些枣椰树品种中常用农药抗氧化性的测定、回收和研究

Gulden Yilmaz, Mustafa Akin, Neslihan Şaki̇
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摘要

在这项研究中,选择了从伊朗、麦地那、突尼斯、耶路撒冷和巴格达等不同国家进口的五种椰枣,以确定椰枣的抗氧化活性特性。此外,还分析了在椰枣植物中使用的 10 种农药残留,并研究了农药残留对恢复使用的影响。用 DPPH 和 Folin-Ciocalteu 酚试剂测定了椰枣提取物的抗氧化活性。采用 LC-MS-MS 技术进行了农药残留研究,并采用 AOAC.2007.01 和 15662 Quechers 方法进行了回收率研究 枣果的抗氧化活性和总酚含量受地点、遗传变异、环境特征、成熟阶段和提取方法的影响。在提取物中测定了大量残留农药。经测定,麦地那椰枣果实中的二氧威克(Dioxacarb)残留量超过了耐受极限。根据 AOAC 2007.01 Quechers 方法,麦地那椰枣中甲基毒死蜱的最高回收率为 57.069。研究发现,与标准抗氧化剂相比,椰枣提取物的抗氧化活性较低。在对椰枣进行的农药分析中,发现了许多农药残留,其中一些超过了规定的限值。无论是从消费者的健康角度,还是从出口食品不能退运的角度来看,事先确定食品中的农药残留量并不超过容许限度都是非常重要的。在研究范围内,对枣 果中常用的农药残留进行了分析和测定。
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Bazı Hurma Çeşitlerinde Yaygın Olarak Kullanılan Pestisitlerin Belirlenmesi, Geri Kazanımı ve Antioksidan özelliklerinin Araştırılması
In this study, five types of dates imported from different countries, namely Iran, Medina, Tunisia, Jerusalem, and Baghdad, were selected to determine the antioxidant activity properties of dates. In addition, 10 pesticide residues used in date plants were analyzed and the effects of pesticide residues on recovery using were investigated. Antioxidant activities of the date extracts were determined by using DPPH and Folin–Ciocalteu phenol reagent assays. Pesticide residue studies were performed by using LC-MS-MS technique and recovery studies were carried out by using AOAC.2007.01 and 15662 Quechers methods Antioxidant activity and total phenol contents of date fruit were affected by location, genetic variability, environmental characteristics, maturation stages, and extraction methods. A lot of residual pesticides were determined in the extracts. It was determined that the Dioxacarb residue in the Medina date fruit was above the tolerance limit. According to AOAC 2007.01 Quechers method, the highest recovery of Chlorpyrifos Methylin was found as 57.069 in Medina date. In the study, it was determined that date extracts showed lower antioxidant activity compared to standard antioxidants. Many pesticide residues were detected in the pesticide analyzes made on dates, and some of them were found to be above the specified limits. It is of great importance that the pesticide residue amounts in foodstuffs are determined beforehand and not exceed the tolerance limits, both in terms of consumer health and in terms of not returning the exported food products. Within the scope of the study, pesticide residues commonly used in Date fruit were analyzed and determined.
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