基于粉末颗粒形状和固体负载的金属注射成型原料流变学研究

Widyastuti Widyastuti, Budi Agung Kurniawan, Adhy Prihatmiko Wibowo, Eka Nurul Falah, Sugiarto Putra Wijaya, Afrizal Aditya Pratama, Ninik Safrida, Faizah Ali
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摘要

金属注射成型(MIM)原料由铜粉和复杂的粘合剂系统组成,粘合剂系统由 PA6、MgSt 和 GMS 组成,固含量(43-53vol%)各不相同。所使用的铜粉末是通过气体和水雾化制造的。所用的粉末颗粒形状有球形和树枝状两种。通过扫描电子显微镜(SEM)可以确定颗粒的球形度。流变学测试用于确保最佳的固体装载量,并研究颗粒形状的影响。在所有工作温度下,所有原料都表现出假塑性,粘度随着剪切速率的增加而降低。本研究中,原料的粘度、流动活化能和流动行为指数等流变学测试结果表明,最佳固体添加量为 43vol%。气体和水雾化粉末都是理想的 MIM 原料。根据流变行为测试,球形气雾化粉末比树枝状水雾化粉末具有更好的流变稳定性。选择了合适的 MIM 原料,气雾化粉末的固含量为 43%。
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Rheology Investigation of Metal Injection Molding Feedstock Based on Powder Particle Shape and Solid Loading
Metal injection molding (MIM) feedstock is composed of Cu powder and a complex binder system that consists of PA6, MgSt, and GMS with various solid loading (43-53vol%). Cu powders used are fabricated by gas and water atomization. Powder particle shapes used have spherical and dendritic shapes. Sphericity of particles can be identified by Scanning Electron Microscopy (SEM). A rheology test is used to ensure the optimum solid loading and investigate the influence of particle shape. The pseudo-plastic behavior of all the feedstock is exhibited by decreasing viscosity along with increasing shear rate for all working temperatures. In this study, rheological test result such as viscosity, flow activation energy, and flow behavior index of feedstock indicates that the optimum solid loading was selected as 43 vol%. Both gas and water atomized powders are desirable for MIM feedstock. According to the rheology behavior test, gas-atomized powders with spherical shape has better rheology stability than water-atomized powders with dendritic shape. The proper MIM feedstock was selected to solid loading 43 vol% with gas-atomized powders.
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