生态绿色银纳米粒子的制备、表征以及在 6061amc 上的摩擦学增强效果

H. Gassour, G. A. Abu El-Magd, A. Mazen, A. M. Ibrahim
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引用次数: 0

摘要

如今,由于纳米粒子的绿色合成方法具有经济可行性和环境友好性,因此研究人员大多对这种方法情有独钟。与本研究中开发的生态绿色方法相比,传统合成方法有一个明显的缺点:反应时间延长。本研究提出了一种生产银纳米粒子(AgNPs)的新方法,然后将其用于强化 Al6061 合金基体。为了优化新型微波辅助绿色 AgNPs 合成,我们进行了多次试验,以加快反应时间。该方法涉及微波辐照芦荟叶提取物。生产出的纳米粒子被用于研究增强型 Al6061 基质成分的摩擦学特性。XRD 分析表明了颗粒尺寸的改善,尤其是在使用微波辅助方法时,并证实了在新引入的绿色方法中生成了 AgNPs。对指数、原子间距和比表面积进行了分析。采用粉末冶金技术制造了三种 AgNPs 含量分别为 0、1 和 2 wt.进行了干磨损试验,监测了许多试验参数,如温度、摩擦力和湿度。评估了摩擦系数(COF)和重量损失率与摩擦学特性的关系。在不同的滑动速度下,对失重率与 AgNPs 含量之间的关系进行了研究,结果表明,AgNPs 的性能得到了显著改善。
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ECO-GREEN SILVER NANOPARTICLES PREPARATION, CHARACTERIZATION, AND TRIBOLOGICAL ENHANCEMENTS ON 6061AMC
Nowadays, researchers are mostly drawn to green synthesis methods for nanoparticles because of their economic viability and environmental friendliness. Compared to the eco-green approaches developed in this work, traditional synthesis methods have one significant drawback: an extended reaction time. This work presents a novel method for producing silver nanoparticles (AgNPs), which is then used to reinforce Al6061 alloy matrix. For a novel microwave assisted green AgNPs synthesis optimization, many trials have been made to speed up the reaction time. The approach involves microwave-irradiating extracts of Aloe vera leaves. The produced nanoparticles were used to investigate tribological characteristics of the reinforced Al6061matrix composition. XRD analysis demonstrated improvements in particle sizes, particularly when utilizing the microwave-assisted approach, and confirmed the creation of AgNPs in the newly introduced green method. Indexing, inter atomic spacing, and specific surface area, were analyzed. Three samples, 0, 1, and 2 wt. % AgNPs contents, were manufactured using powder metallurgical technique for the purpose of investigating tribological enhancements. A dry wear test was performed monitoring many test parameters such as temperature, friction force, and humidity. The coefficient of friction (COF) and weight loss rates were evaluated in relation to the tribological properties. At different sliding speeds, the relationship between weight loss rates and AgNPs contents was examined, and substantial improved behavior was perceived.
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