浅低温处理(-20 °C)与深低温处理(-196 °C)在提高 Mg/2wt.%CeO2 纳米复合材料性能方面的比较

Shwetabh Gupta, Gururaj Parande, M. Gupta
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摘要

由于镁及其复合材料具有高比强度和低密度的特性,因此被广泛应用于各种领域。然而,由于缺乏对镁合金在零度以下条件下性能的研究,其应用仅限于室温条件。本研究首次尝试了两种低温(-20 °C/253 K 和 -196 °C/77 K)对 Mg/2wt.%CeO2 纳米复合材料的物理、热和机械性能的影响。这些材料采用分解熔融沉积法合成,然后进行热挤压。结果表明,与在 -196 °C 的液氮中进行深度低温处理的样品相比,浅度低温处理(-20 °C冷藏)的样品孔隙率降低,耐燃性降低,微硬度、压缩屈服度、极限强度和破坏应变相似。虽然经深度低温处理的样品显示出整体优势,但由于在零下 20 ℃ 暴露的样品显示出非常相似的机械性能,从而降低了低温处理的整体成本,因此性能提高的程度可能并不合理。研究结果与公开文献中的数据进行了比较,并对性能改善背后的机理进行了评估。
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Comparison of Shallow (−20 °C) and Deep Cryogenic Treatment (−196 °C) to Enhance the Properties of a Mg/2wt.%CeO2 Nanocomposite
Magnesium and its composites have been used in various applications owing to their high specific strength properties and low density. However, the application is limited to room-temperature conditions owing to the lack of research available on the ability of magnesium alloys to perform in sub-zero conditions. The present study attempted, for the first time, the effects of two cryogenic temperatures (−20 °C/253 K and −196 °C/77 K) on the physical, thermal, and mechanical properties of a Mg/2wt.%CeO2 nanocomposite. The materials were synthesized using the disintegrated melt deposition method followed by hot extrusion. The results revealed that the shallow cryogenically treated (refrigerated at −20 °C) samples display a reduction in porosity, lower ignition resistance, similar microhardness, compressive yield, and ultimate strength and failure strain when compared to deep cryogenically treated samples in liquid nitrogen at −196 °C. Although deep cryogenically treated samples showed an overall edge, the extent of the increase in properties may not be justified, as samples exposed at −20 °C display very similar mechanical properties, thus reducing the overall cost of the cryogenic process. The results were compared with the data available in the open literature, and the mechanisms behind the improvement of the properties were evaluated.
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