对 PBF-LB AlSi10Mg 合金进行直接人工老化,以加强强度和残余应力消除之间的权衡

Gianluca Di Egidio, Lavinia Tonelli, Mattia Zanni, Daniele Carosi, Alessandro Morri, Lorella Ceschini
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引用次数: 0

摘要

AlSi10Mg 合金是通过粉末床熔融-激光束(PBF-LB)加工的合金中研究最多的一种。许多已发表的研究都集中在减少残余应力或提高机械强度的后处理热处理上。而本研究的目的是找出能够优化这两方面的直接人工时效(AA)热处理方法,从而提高使用免加热平台生产的 PBF-LB AlSi10Mg 合金在强化和消除残余应力之间的权衡。根据热分析结果,选择了比 AA 热处理通常使用的温度(190-240 °C)更高的温度,这样既有利于消除残余应力,又有利于从析出合金的过饱和固溶体中析出强化相。通过绘制老化曲线以及 XRD 和拉曼分析,评估了 AA 热处理对机械性能(即硬度)和残余应力的影响,结果表明通过调整热处理参数(温度和时间)可以在强化和消除应力之间实现不同的权衡。特别是,在最低温度(190 °C)下暴露会导致残余应力部分减小,硬度略有增加。通过提高热处理温度和增加浸泡时间,残余应力得到了更明显的缓解,而硬度的降低则相当有限。由于采用了不同的热处理条件,在样品上观察到的微观结构变化支持了这些结果,并显示了为 PBF-LB AlSi10Mg 合金设计 AA 热处理的可行性,这种热处理能够满足最终应用所需的机械响应。
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Direct artificial aging of the PBF-LB AlSi10Mg alloy designed to enhance the trade-off between strength and residual stress relief

The AlSi10Mg alloy is one of the most studied alloys processed by the Powder Bed Fusion-Laser Beam (PBF-LB). Many already published works focus on post-process heat treatments to reduce residual stress or improve mechanical strength. Instead, the present study aims to identify direct artificial aging (AA) heat treatment able to optimize both aspects, thus enhancing the trade-off between strengthening and residual stress relief for the PBF-LB AlSi10Mg alloy produced using a no-heated platform. Higher temperatures (190–240 °C) than those typically used in AA heat treatment were selected based on thermal analysis to benefit both residual stress relief and precipitation of reinforcing phases from the supersaturated solid solution of the metastable as-built alloy. The effects of AA heat treatment on mechanical properties (i.e. hardness) and residual stress were evaluated by plotting aging curves and by XRD and Raman analyses and demonstrated that different trade-offs between strengthening and stress relief can be achieved by tuning heat treatment parameters (temperature and time). In particular, the exposure at the lowest temperature (190 °C) induced a partial decrease in residual stress and a slight increase in hardness. By increasing heat treatment temperature and soaking time, the relief was more significant, whilst the decrease in hardness was rather limited. The results are supported by the microstructural changes observed on the samples due to the different heat treatment conditions applied and show the feasibility of designing an AA heat treatment for the PBF-LB AlSi10Mg alloy capable of satisfying the mechanical response required by the final application.

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