测定城市水体中有机污染的色谱法:最新小型综述。

IF 4.2 2区 化学 Q1 CHEMISTRY, ANALYTICAL Critical reviews in analytical chemistry Pub Date : 2024-03-07 DOI:10.1080/10408347.2024.2318764
Paulina Gątarek, Angelina Rosiak, Joanna Kałużna-Czaplińska
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引用次数: 0

摘要

有可能进入环境中的污染物和化学品的数量在很大程度上仍是未知数,这给各科学领域的研究人员、环境科学家和分析化学家带来了巨大挑战。色谱技术,包括气相色谱(GC)和液相色谱(LC),再加上不同类型的检测,现已成为鉴定水中各种化合物和污染物的宝贵工具。本综述主要介绍过去几年发表在科学文献中的用于测定水生介质(主要是城市水体)中新出现的有机污染物的色谱技术:GC-MS、GC-Orbitrap-MS、GC-MS/MS、GC-HRMS、GC × GC-TOFMS、GC-ECD、LC-MS/MS、HPLC-UV、HPLC-PDA、UPLC-QTOFMS。文章还重点介绍了用于分析水样的样品制备方法。大多数研究的重点是尽量减少样品制备步骤、减少溶剂用量、提高分析速度以及将其应用于样品中多种分析物的能力。这对于应用灵敏的选择性方法监测城市水质状况和评估其对人类健康的影响极为重要。
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Chromatographic Methods for the Determination of Organic Pollution in Urban Water: A Current Mini Review.

The number of pollutants and chemicals with the potential to reach the environment is still largely unknown, which poses great challenges for researchers in various fields of science, environmental scientists, and analytical chemists. Chromatographic techniques, both gas chromatography (GC) and liquid chromatography (LC) coupled with different types of detection, are now invaluable tools for the identification of a wide range of chemical compounds and contaminants in water. This review is devoted to chromatographic techniques GC-MS, GC-Orbitrap-MS, GC-MS/MS, GC-HRMS, GC × GC-TOFMS, GC-ECD, LC-MS/MS, HPLC-UV, HPLC-PDA, UPLC-QTOFMS, used to determinate emerging organic contaminants in aquatic media, mainly in urban water, published in the scientific literature over the past several years. The article also focuses on sample preparation methods used in the analysis of aqueous samples. Most research focuses on minimizing the number of sample preparation steps, reducing the amount of solvents used, the speed of analysis, and the ability to apply it to a wide range of analytes in a sample. This is extremely important in the application of sensitive and selective methods to monitor the status of urban water quality and assess its impact on human health.

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来源期刊
CiteScore
12.00
自引率
4.00%
发文量
137
审稿时长
6 months
期刊介绍: Critical Reviews in Analytical Chemistry continues to be a dependable resource for both the expert and the student by providing in-depth, scholarly, insightful reviews of important topics within the discipline of analytical chemistry and related measurement sciences. The journal exclusively publishes review articles that illuminate the underlying science, that evaluate the field''s status by putting recent developments into proper perspective and context, and that speculate on possible future developments. A limited number of articles are of a "tutorial" format written by experts for scientists seeking introduction or clarification in a new area. This journal serves as a forum for linking various underlying components in broad and interdisciplinary means, while maintaining balance between applied and fundamental research. Topics we are interested in receiving reviews on are the following: · chemical analysis; · instrumentation; · chemometrics; · analytical biochemistry; · medicinal analysis; · forensics; · environmental sciences; · applied physics; · and material science.
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