研究和应用不同的提取技术生产更细的竹纤维

Fisseha Wubneh Asmare , Xiaodong Liu , Guanfang Qiao , Ruixia Li , Murugesh Babu K , Dacheng Wu
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引用次数: 0

摘要

竹子是重要的纤维来源。天然竹纤维具有可用于纺织品的特性。然而,由于难以提取较细的纤维,竹纤维尚未得到应有的重视。要充分利用竹子的潜力,就必须采用先进的技术提取竹纤维。在这项研究中,开发了三种不同的提取方法,利用新创建的复合酶和碱的组合来提取更细的天然竹纤维。新酶以固态和液态两种形式应用。在制备竹秆和提取纤维时,还采用了机械工艺。该研究使用了三种常见的竹子,即峨眉簕竹(Neosinocalamus affinis)、箬竹(Phyllostachys heterocycla)和网纹竹(Phyllostachys bambusoides)来提取天然竹纤维。竹子样品用 3-6% 的碱和 24-36% 的复合酶(按重量计算)进行处理。复合酶是最近开发的一种酶,以液态和固态两种形式使用,无需水作为溶剂(非水处理)。对所得纤维的物理特性(如含水量、长度和细度)和机械(拉伸)特性(如断裂韧性、断裂负荷和断裂伸长)进行了评估,并得出了其最小值、最大值和平均值。使用红外光谱(FTIR)、X 射线衍射(XRD)、热分析仪(TGA)和扫描电子显微镜(SEM)进行了结构分析。此外,还测定了竹纤维的产量百分比。竹纤维的含水量为 7.32-7.71%,平均长度为 5.48-6.01 厘米,线密度为 9.71-11.43 tex,断裂载荷为 138.96-147.67 cN,断裂韧性为 12.16-15.21 cN/tex,断裂伸长率为 2.60-2.75%。扫描电子显微镜、热重分析和傅立叶变换红外光谱测试表明,这些纤维不是单一的纤维素纤维,而是由木质素和半纤维素粘合在一起的纤维束。热重分析结果表明,纤维的热稳定性足以承受高温纺织工艺。XRD 结果表明,由于部分去除了非结晶木质素和其他成分,天然竹纤维的结晶度有所提高。测得的纤维特性标准偏差值为 0.36-2.52,表明每个样品的均匀度很高。实验结果表明,本研究获得的纤维具有用于纺织品的潜力。纤维产量百分比(约为 52.7%-55.2%)证实了这三种竹子都有提供可用纤维的潜力。
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Investigation and application of different extraction techniques for the production of finer bamboo fibres

Bamboos are an important source of fibres. Natural bamboo fibres possess have characteristics that make them of potential use in textiles. However, they have not received the attention they deserve due to the difficulty of extracting finer fibres. Full utilization of the potential of bamboo requires the extraction of the fibres using advanced techniques. In this study, three different extraction methods were developed, utilizing a newly created composite enzyme and alkalis in combination to extract finer natural bamboo fibres. The new enzyme was applied in both a solid form and a liquid state. Mechanical processes were also employed in preparing the bamboo culms and extracting the fibres. Three commonly grown bamboo species, Bambusa emeiensis (Neosinocalamus affinis), Phyllostachys edulis (Phyllostachys heterocycla), and Phyllostachys reticulata (Phyllostachys bambusoides), were used in the study to extract natural bamboo fibres. The bamboo samples were treated with 3–6% alkali and 24–36% composite enzyme, based on their weight. The composite enzyme was a recently developed enzyme that was used in both a liquid form and a solid form without the need for water as a solvent (non-aqueous treatment). The physical properties such as moisture content, length and fineness, and mechanical (tensile) properties such as breaking tenacity, breaking load and breaking extension of the resulting fibres were assessed with their minimum, maximum and average values. Structural analyses were performed using infrared spectroscopy (FTIR), X-ray diffraction (XRD), thermal analyzer (TGA) and scanning electron microscopy (SEM). The yield percentages of bamboo fibres were also determined. The bamboo fibres had a moisture content of 7.32–7.71%, an average length of 5.48–6.01 cm, a linear density of 9.71–11.43 tex, a breaking load of 138.96–147.67 cN, a breaking tenacity of 12.16–15.21 cN/tex, and a breaking elongation of 2.60–2.75%. SEM, TGA and FTIR tests indicated that the fibres were not single cellulosic fibres but rather fibre bundles in which single fibres were bonded by lignin and hemicellulose. The TGA results showed that the fibres were sufficiently thermally stable to withstand high temperature textile processes. The XRD results indicated the improvement of the crystallinity of the natural bamboo fibres owing to the partial removal of the non-crystalline lignin and other components. The measured properties of the fibres showed standard deviation values of 0.36–2.52, indicating a high level of uniformity within each sample. The experimental results demonstrated that the fibres obtained in this study have the potential to be used in textiles. The fibre yield percentages (approximately 52.7–55.2%) confirmed that all three bamboo species have the potential to provide usable fibres.

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