{"title":"MnFe2O4 纳米粒子作为一种新型磁分离纳米催化剂,用于无溶剂合成二氢吡喃 [2,3-c] 吡唑衍生物","authors":"Santosh B. Gaikwad, Kishore Puri","doi":"10.32628/ijsrst173876","DOIUrl":null,"url":null,"abstract":"This study focused on synthesising MnFe2O4 (Manganese Ferrite) nanoparticles using the sol-gel method. We then applied these nanoparticles as a catalyst for synthesising dihydropyrano[2,3-c]pyrazole derivatives at a specific temperature. The significant advantage of this process is that it requires only short reaction times and no solvents. Additionally, the crude pyranopyrazole derivatives can be purified through a simple recrystallization process. The catalyst is reusable, magnetically separable and maintains its activity even after five uses. The chemical integrity of the catalyst was confirmed through FT-IR, 1H NMR, and 13C NMR techniques.","PeriodicalId":14387,"journal":{"name":"International Journal of Scientific Research in Science and Technology","volume":"39 3","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2024-01-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"MnFe2O4 nanoparticle as a new and magnetically separable nanocatalyst for solvent-free synthesis of dihydropyrano [2,3-c]pyrazole derivatives\",\"authors\":\"Santosh B. Gaikwad, Kishore Puri\",\"doi\":\"10.32628/ijsrst173876\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"This study focused on synthesising MnFe2O4 (Manganese Ferrite) nanoparticles using the sol-gel method. We then applied these nanoparticles as a catalyst for synthesising dihydropyrano[2,3-c]pyrazole derivatives at a specific temperature. The significant advantage of this process is that it requires only short reaction times and no solvents. Additionally, the crude pyranopyrazole derivatives can be purified through a simple recrystallization process. The catalyst is reusable, magnetically separable and maintains its activity even after five uses. The chemical integrity of the catalyst was confirmed through FT-IR, 1H NMR, and 13C NMR techniques.\",\"PeriodicalId\":14387,\"journal\":{\"name\":\"International Journal of Scientific Research in Science and Technology\",\"volume\":\"39 3\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2024-01-22\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Scientific Research in Science and Technology\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.32628/ijsrst173876\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Scientific Research in Science and Technology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.32628/ijsrst173876","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
MnFe2O4 nanoparticle as a new and magnetically separable nanocatalyst for solvent-free synthesis of dihydropyrano [2,3-c]pyrazole derivatives
This study focused on synthesising MnFe2O4 (Manganese Ferrite) nanoparticles using the sol-gel method. We then applied these nanoparticles as a catalyst for synthesising dihydropyrano[2,3-c]pyrazole derivatives at a specific temperature. The significant advantage of this process is that it requires only short reaction times and no solvents. Additionally, the crude pyranopyrazole derivatives can be purified through a simple recrystallization process. The catalyst is reusable, magnetically separable and maintains its activity even after five uses. The chemical integrity of the catalyst was confirmed through FT-IR, 1H NMR, and 13C NMR techniques.